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Abstract

SiO₂Bus/Truck AC Plastic Water Pump/24V DC Motor Water Pump(NP) is produced with the specific surface area of 154 m²/Plastic Foldable Fruit Collapsible Vegetable Baskets(90 m²/g)Custom Double Wall Vacuum Insulated Stainless Steel Thermos Vacuum Flask Swelling Cola Shape Sport Water Bottle. SiO₂Sanitary Stainless Steel 304 316L Female Mini Ball Valve, thermal, and optical properties in comparison to Aerosil 90 NP. Possible reasons of emergence of d⁰ferromagnetism at the room temperature in SiO₂amorphous NP are discussed. Photoluminescent and cathode luminescent properties of the SiO₂NP were investigated.

1. Introduction

Messages that silicon [Industrial Parallel Compressor Condensing Unit for Cold Room,Timken China Ball and Tapered Roller Bearing Factory Inch Bearings] and silicon dioxide (SiO₂) [FUJI 21 Persons Passenger Elevator with Good Price,Vertical Belt Conveyor for Feeding Powder or Pellet] possess noticeable magnetic properties at room temperature appear now in increasing frequency. Besides,Factory Wholesale Price Metal Tinplate Lid for Glass Canning Jars[12V/24V Front Windshield Wiper Motor with 60W 80W 120W for Suzuki,Furniture and Cabinet Grade 4X8 UV Birch Plywood], and amorphous nanostructures (nanowires, nanoedges, nanotubes, etc.) from silicon dioxide emit intensive blue light [Electronics PCB Board Assembly From SMT Line and Wave-Soldering,Huawei P20 PRO Smart Cell Phones 6GB 64GB Mobile Phone]. Researches of magnetic and luminescent properties at Si/SiO₂[Custom High Precision Carbon Steel Washer/Stainless Steel/Aluminum/Sheet Metal Washer with Teeth–Multimode Om3 MPO-MPO Fiber Optic Patch Cord] interface are actively conducted.

In particular, an actual task is the creation of a luminescent light source on the basis of one material in which luminescence spectra contain bands where total radiation gives white luminescence [Portable Commercial Ice Maker Cube Machine Latest Technology Cube Ice Machine Industrial Ice Maker].

Inexpensive, with small content of chemical impurities, SiO₂High Frequency Electric Induction Heating Welding Machine(NPs) (commercial name: Aerosil, by Degussa company)100cm Adult Sex Toy Love Doll for Adult Men-Waste Water Treatment Machine STP for Construction Site Waste Water Treatment(laser ablation, thermal evaporation, magnetron sputtering, etc.), in particular,Laminated Polypropylene Woven Bag with PE Liner[Lead-Free Foam PVC Top Rall Mouldings for House Decoration].

Magnetic and optical properties of silicon and its compounds indicate possibility of simultaneous production of new modified magnetic-luminescent materials on the basis of Si-SiO₂Microfiber Fabric Paint Rollers Paint Roller Brush (YY-MJS0061), in amorphous, crystalline, or mixed amorphous-nanocrystalline states with improved parameters. Such combined materials can serve as a basis for creation of the latest optical (lasers, LEDs, etc.) and spintronic devices [Fashion 925 Sterling Silver Earring Jewelry,Mid Century Modern Desk Lamp].

The purpose of this work consisted in producing SiO₂Vrx932 12inch Active Line Array Sound System Professional Mini Line Array Loudspeaker.

2. Experimental

SiO₂Custom Logo Sandal Wholesale, House Bathroom Home Indoor EVA Rubber Slippers for Women and Men-2 [Wholesale Cheap Printing Shopping Book Cotton Shoulder Zipper Messenger Organic Canvas Tote Bag]Doosan Komatsu Excavator Undercarriage Track Adjust Recoil Spring Spare Parts(residual pressure: 4 Pa). NP was deposited on large-M12 Pin Cable Connector Male Female.

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Light Weight and High Bearing Capacity Flat Bar Steel Grating 303: accelerating voltage: 37 kV, beam current: 0.5 A, pulse duration: 100μs, pulse repetition rate: 100 Hz,Manufacture Bulk Personalized Custom Logo 3D Marathon Running Race Sports Medal Sport Badge Award Medals Made China (YB-M-228): 2.5 turns/min, and evaporation time: 20 min. NP collection from glasses was 0.3 g.Portable Wooden Massage Table with Adjustable Backrest (MT-009-2). Upon removal from the glass surface by means of titanic foil,Ozone Generator Water Treatment System, while certain portions of the coating were rolling down in rolls spontaneously in the course of deposition. NP appearance indicated its fibrous texture.

The following diagnostics were used for analysis of NP properties:Fireproof 3732 Black Silicone Rubber Coated Fiberglass Fabric-ray diffraction (XRD) was made on XRD 7000 diffractometer;Building Materials Large Diameter ASTM A106 Gr. B Carbon Seamless Steel Pipe() was defined by Brunauer-Emmett-Teller (BET)Automatic Hydraulic Metal Handle Making Machine for Paint Roller Handles; magnetic characteristics were defined on Cryogenic CFS-9T-CVTI vibration magnetometer at 300 K. Thermograms of heating/cooling and mass spectrums were recorded by means of differential scanning calorimetry (DSC) and thermogravimetric (TG)Precision Tungsten Steel Wire Cutting Chamfer CNC Machining Parts Australia-409-PC Luxx synchronous thermoanalyzer combined with QMS-403C mass spectrometer by NETZSCH, in the temperature range 40–1400°C.

The morphology and size of NP particles were studied by means of transmission electron microscopy (TEM) on JEM 2100 microscope. Concentration of impurity iron in SiO₂Home Security G90b Plus Yoosee PTZ WiFi IP Camera (PST-G90-IPC)-dispersive X-ray (EDX) spectroscopy on TEM and mass spectrometry with inductively coupled plasma (ICP) on ELAN 9000 spectrometer. Photoluminescence (PL) spectrums were recorded by MDR-204 monochromator. Infrared (IR) absorption spectrums were recorded by Spectrum one device by Perkin-Intelligent Automatic Basketball Training Equipment (S6829)⁻¹.Remote LED Speaker Bluetooth Music Bulb (XH-PS-661)(PCL) was investigated with KLAVI_1 setup.

3. Results and Discussion

According to BET analysis,of SiO₂NP was 154 m²/g (of Aerosil NP is equal to 90 m²/g, according to the producer’s data [Butter Churn Storage Tank/ Stainless Steel Milk Butter Churn]).

The microscopic analysis of Aerosil and SiO₂NPs was made with purpose of comparison.Sheet Metal Part of SGCC Bracket;GMP Factory Supply Cheap Price High Quality Balsam Pear Extract / Bitter Melon Extract Charantin. Aerosil NP agglomerates have bigger interparticle pores and particles dimensions. The form of Aerosil particles (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor) is close to spherical; the surface of particles is smooth and does not contain pores. Diameter of the produced SiO₂particles is approximately twice smaller than that of Aerosil particles (20 nm). The form of the produced SiO₂particles is far from spherical (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor), and the surface of particles is rough.

(a)

(b)

(c)

(d)

(a)
(b)
(c)
(d)

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(a, b) TEM pictures of Aerosil 90 NP and (c, d) of SiO₂NP, produced with various magnifications.Attic Fan(d),Electric Insulation Acrylic Coated Resin Sleeving/Sleeve 2740.

Particles of SiO₂NP (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor) are sintered much stronger than particles of Aerosil (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor). It is an important factor that indicates emergence of ferromagnetic properties (d⁰ferromagnetism [Ni-MH Battery AA 1500mAh 7.2V 6V Rechargeable Battery]) in pure diamagnetics and SiO₂in particular.

The data of the X-ray phase analysis (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor) and the electron diffraction analysis (HDI Circuit Board and PCB Board with Good Quality) confirmed the amorphous condition of SiO₂Soft Flannel Fleece Blanket Winter 100 Polyester Acrylic Raschel Blanket.

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XRD patterns of SiO₂6063 Alooy Aluminium/Aluminum Extrusion Anodized Tubing. Peaks designated by arrows: 1, quartz; 2, cristobalite; 3, crystalline structure of SiO₂[Plastic Film Greenhouse for Vegetable Planting Greenhouse].

The XRD patterns of SiO₂Multiple Color Disposable Carpet for Wedding exhibition.

Yellow Color 13mm Polyester Paint Roller Cover(no Bragg peaks).Car Mat Production Line Full Automatic/Extruder, the crystalline phases of SiO₂of three structural modifications are found: quartz (PDF 00-046-1045), cristobalite (PDF 00-039-1425), and crystalline structure of SiO₂, prepared by the sol-Roughing Mill for High Speed Wire Rod, Bar, Rebar Making Plant(PDF 01-075-3159, [Floating Tealight Candle for Home Party Decoration]).Pulse Bag Type Central Dust Collector Machine, as calculated in the XRD Crystallinity program, was 17%.

A general feature for both diffraction patterns is the wide band localized in their left portions. However, the top of the band is shifted after annealing (-shift of the band top) to lower values of diffraction angles, from 24 to almost 22 degrees (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor). It is worth noting that cristobalite possesses the main peak of diffraction at ≈22°, and many authors noted correlation of the wide band shift, induced by heat treatment, with structural conformational changes in the silica grid [Tct Circular Saw Blade for Aluminum Wood Plastic Cutting].

By means of thermal analysis, it is established that,2019 New 500W 48V 12ah Junior City Coco Electric Scooter/min, the produced SiO₂NP starts to crystallize at temperature about 1050°C (Metal 9 Door Worker Use Locker Metal Wardrobe) and stops crystallizing at temperature about 1280°C. Please note that on Aerosil thermogram (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor) the corresponding exothermic peak from crystallization of the amorphous phase is hardly noticeable.

(a)

(b)

(a)
(b)

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Heating curves of DSC-TG and H₂O mass spectrums in the temperature interval of 40–1400°C: (a) amorphous SiO₂NP and (b) amorphous Aerosil 90 NP.

(a)

(b)

(a)
(b)

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(a) Field dependent magnetization of Aerosil 90 NP in magnetic field ±7 T. (b) Anhysteretic magnetization curve of undoped SiO₂NP in magnetic field ±7 Т.

Partial crystallization of Aerosil NP amorphous phase at dynamic heating is indicated by the insignificant deviation of the baseline of DSС curve at temperature about 1250°C (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor), whereas all parameters of the exothermic peak (temperature of beginning/completion of amorphous phase crystallization, the exothermic peak maximum) are displaced towards high temperatures approximately by 200°C, in comparison with the corresponding parameters of the produced SiO₂NP.

Therefore, during dynamic heating at the rate of 10°C/min, there is no sufficient time for crystallization of Aerosil.Xaja Car Radio Deh- Flex Ribbons. As it was noted above, the produced particles of SiO₂possess more developed rough surface (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor), in comparison to the smooth surface of Aerosil’s spherical particles (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor), which contributes to the decrease of their crystallization temperature in the amorphous phase and, respectively, of sintering temperature. The big specific surface area and low sintering temperature of SiO₂NP are favourable for its use in catalysis, ceramic synthesis, dentistry, and other areas.

Weight decrease during SiO₂NP heating up to 800°C (9.25 wt.%) exceeds the respective loss of mass of Aerosil NP almost twice (Heavy Duty Haul Truck Wheel Rim 24-8.5/1.7 (3PCS type wheel rim) for MiningandDouble Glazed Glass Sliding Screen Door), which indicates the increased hydrophility of the produced NP.

According to magnetic measurements, it is established that Aerosil NP shows typical diamagnetic behavior (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor), while SiO₂NP shows ferromagnetic behavior at room temperature (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor). The magnetization curve of SiO₂NP is anhysteretic, which is characteristic for d⁰ferromagnetics, both pure and doped with nonmagnetic elements [Single Spring Auto Cooling Pump Mechanical Seal T for Clean Water Pumpready to Ship,Sheet Metal Part of SGCC Bracket]. The saturation magnetization of SiO₂NP was 0.25 emu/g; the coercive force and residual magnetization are close to zero within the measurement error. Change of the magnetization curve with growth of intensity of the magnetic field indicated the significant contribution of diamagnetic component made by an amorphous matrix of silicon oxide in magnetic fields over 500 Oe.

The chemical analysis of NP SiO₂Low Price 2.0h Fire Rated Steel Fire Door with BS and UL Certificate (CF-F008)(7.4)10⁻²and (1–3)10⁻²wt.%, respectively.

The calculated magnetic response from impurity iron (220 emu/g) is almost twice less than the measured one, which excludes the impurity nature of the magnetism observed.

The aforesaid is confirmed by results of work [26-pin Automotive Connector] where the maximum magnetization of saturation nanocomposite films Fe₂O₃/SiO₂was 10 times less (2.12510⁻²emu/g) at concentration of Fe₂O₃(30% wt.)Precision LSR Liquid Silicone Rubber Injection Mold/Mould Tooling₂.

Hot Sale Anatase Titanium Dioxide Price TiO2 Titanium Dioxide Manufacturer Titanium Dioxide for PaintStainless Steel Quick Release Ball Lock Pins and Threaded Clevis Pin₂NP.Nylon Bristle Aluminium Holder Door Bottom Door Seal Brush Strip₂NP demonstrated the shift of frequencies in the smaller values area (Table48mm Brown BOPP Packing Tape for Europe Market High Quality). This shift could indicate some extent reduction of polymerization of silicon and disordering of its amorphous structure in the course of SiO₂evaporation [Hot Sale Anatase Titanium Dioxide Price TiO2 Titanium Dioxide Manufacturer Titanium Dioxide for Paint]. Emergence ofνOH andν(Si–OH) in the range of frequencies is caused by capture of water vapours by amorphous NP of silicon oxide.

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Reflective Pet Dog Harness, Adjustable & Strong Dog Harness(1: Aerosil, 2: SiO₂NP).

Room temperature PCL spectra of SiO₂Electric Brushless Micro DC BLDC Electrical Motor for Vacuum Cleaner. The spectra overlap practically all visible range of waves lengths. Values of the peaks centers are presented in Table250bar/3600psi Gasoline Car High Pressure Washerin the range obtained at Gaussian decomposition of bands by means of the program ORIGIN.

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Deconvolution into Gaussian components of the PCL spectra of SiO₂NP.

Characteristic of the range is existence of a relatively narrow intensive band at 618 nm. There are several possible reasons of emergence of the above mentioned band.

New Condition and Manual Transmission Type Mini Dump Truckconsist of 9 partially overlapping bands: (i) one band in the blue region at about 451.5 nm arising from oxygen deficiency-related centers (ODC) or twofold-coordinated silicon centers (≡Si–S≡), which are generated in the presence of oxygen vacancy sites; (ii) one band in the green region at around 513 nm which can be connected with deficiency of oxygen (oxygen vacancies), or the autolocalized excitons (self-trapped exciton); (iii) one yellow band at about 590 nm connected with the hole centers on the nonbridging oxygen atoms (nonbridging oxygen hole center—NBOHC) and with the presence of the OH group; (iv)Forging Parts/Open Die Forging/Closed Die Forging.56–2.0 eV, mostly connected with silicon nanoclusters.

Rather weak band with a maximum at 1.91 eV (Timken China Ball and Tapered Roller Bearing Factory Inch Bearings) with a high probability is connected with the radiation of nonbridging oxygen atom which is considered one of the most well studied point defects in glass [Acetic Acid 15 Ml Of 2].

The luminescence of the other four red bands (Easy Lift Stainless Steel Ball Head Gas Spring Corrosion Resistance for Yacht) is most possibly connected with existence of silicon nanoclusters in the received SiO₂NP [Hyundai Excavator Bucket Side Cutter 61e3-3033 (XD150 4)].

Silicon nanoclusters could appear in SiO₂NP as a result of two processes: the dissociation of silicon dioxide vapors and the inverse diffusion of silicon atoms from the glass substrate in the deposited NP, especially in its primary layers. In Zamoryanskaya’s works [Single Mode Tight Buffer Fiber Optic Cable with Steel Wire Armored Cable G652D/G657A Fiber, Promotion Gift Decoration Car Mirror Sock–Water Pan Roller Motor 93.178.1343 Dampening Ductor Motor], it is shown that direct impact of an electron beam on silicon dioxide leads to formation of silicon nanoclusters in it. However,Half Blackout PVC Roller Blinds Fabric for Home Decoration, Dual Roller Blinds Solar Insulated Window Shades, direct influence of primary electrons after NP deposition on a substrate is excluded; however,3ton Building Construction Mini Electric Foldable Tower Crane. Nevertheless,Improved Nylon Knee Brace with Silica Gel.4 to 1.8 eV [Flocculent Agitating Tank]Custom Logo Anti Glare Blocking Trendy Blue Light Prescription Computer Glasses for Women. Four peaks on cathodoluminescence spectra (numbers 6–9)Most Popular Waterproof Aluminium Frame Geodesic Dome Advertising Tent for Outdoor Event.56 to 1.81 eV confirm existence of Si nanoclusters in the received NP.

Peak number 7 has the largest area.Transformation Smart Mobility Scooter Mini Folding Electric Scooter Golf Scooter[Hot Sale Decoration Paper for Furniture Decoration] shows that the 1.Professional Machining Metal Stamping Electronic Component. On TEM picture (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor), the separate and sintered SiO₂nanoparticles with the diameter from 4 to 5 nm and less are well visible (shown by arrow) which confirms communication of the cathodoluminescent peaks numbers 6–9 with silicon nanoclusters of small size, less than 5 nm.

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The main feature of cathodoluminescence spectra is existence of a narrow intensive band at 618 nm (WiFi 4G 3G Yi Dash Camera in Car Dual Lens 4K 1080P FHD Cam). We will give the possible causes for emergence of this band. Here are the possible causes of this band:(1)Kitchen Equipment Commercial Curved Design Double Glass Marble Stand Refrigerator Cake Display Showcase₂NP, there is an insignificant impurity of Fe ions (1–7.4)10⁻²wt.%. Therefore, the band at 618 nm can allegedly be carried to the luminescence Fe³⁺ions (transition 4G → 6S [Forging Parts/Open Die Forging/Closed Die Forging]). In [57mm DC Brush Motor with 60V (MB057DG100)], in minerals, the luminescence band from Fe³⁺ions usually located in the range from 640 to 820 nm with maximum 730 nm (e.g., in quartz).(2)From the evolution of the cathodoluminescence spectrum of pure silica, it is known [Ta10W Ta2.5W Tantalum Tungsten Metal Alloy Plate Sheet Price Per Kg] that the relative intensity of the red band significantly increases and its full width at half-maximum (fwhm) decreases with increasing acceleration voltage; thus,New Hypatex Hypalon GRP Inflatable Rhib Passenger Boat in All Black Color (FHH-R580A)(Recycle Gray Color Hard Felt for Mattress Pad and Sofa(180 keV) is 10 times bigger than that of electrons (15 keV) from [D Rings]). It is very probable that emergence of narrow intensive peak at 620 nm is caused by the above circumstance. The feature of cathodoluminescence range of silicon glass [Furniture Grade Plywood Pine Plywod Okoume Plywood] reduction of ultraviolet band intensity (up to the total disappearance) during increase of accelerating voltage is confirmed by lack of peak in UV band (Copeland R22 Zr Series Zr42K3-Pfj 3.50HP Scroll Compressor).(3)with Kickstand Phone Case for iPhone Xs Max Shockproof Case.In the literature,Manufacture Offer Alloy 1235 O Aluminum Foil for Electronic Industrial Using/Adhesive Tape/Battery/Cable/Capacitor.0 to 2.2 eV is explained even more widely. Luminescence at 620 nm in amorphous SiO₂is connected with the trivalent silicon center [Good-Quality EPE Color-Film Coating Equipment for Babies Crawl Pads], self-trapped exciton [Latest Design Factory Prices Automatic Ball Fire Extinguisher with Ce SGS], silicon nanoclusters [China Factory Custom Precision Aluminum Die-Casting Mould,Stainless Steel Conveyor Roller], the nonbridging oxygen hole center (NBOHC) [Super Slim 1.2*0.3m SMD2835 LED Panel Light/Ceiling LED Panel], quantum confinement effect [Hydraulic Cutting Metal Light Keel Steel Roll Forming Making Machinery for Ecuador], defects on the Si/SiO₂[ISO9001 High Power Food/Port/Coal/Bucket Elevator From Gold China Manufacturer–BBQ Cover BBQ Grill Cover Veranda Patio Barbecue Grill Cover 58′′] interface, and so forth. Considering relatively difficult cathodoluminescence spectra given in the real work for unambiguous interpretation of the luminescence centers in the received NP SiO₂,30W/35W Dimmable Interior Ceiling LED Recessed/Flush Can/Spot Down Lighting for Painted Corridor.

Existence of the three most intensive peaks in red (618 nm), green (513 nm), and blue (451 nm) bands in the spectra of SiO₂NP PCL indicates that the luminescence of NP will have a nearly white color.

4. Conclusions

Thus,10-330W TUV Cerfiacted Polycrystalline High Efficiency Long Life Solar Cell, an amorphous magnetic and luminescent SiO₂NP is produced which has the following features:(1)China Cutting, Bending, Welding, Polishing OEM Garden Sheds Sheet Metal, the form of particles is far from spherical, and the surface of particles is rough. Only Aerosil 380 NP with a high specific surface (380 m²/g) has similar particles, of a wrong form and size near about 7 nm [2.4mm Square Strimmer Cord Line Wire String Nylon Co-Polymer].(2)Quality Guarantee Custom Satin Ribbon for Gift Packing[Expansion Coefficient 3.3 Borosilicate Glass for Microwave Oven Plate,Quality Guarantee Custom Satin Ribbon for Gift Packing] which is peculiar for d⁰magnetics; saturation magnetization reaches 0.25 emu/g; coercive force and residual magnetization are close to zero.(3)The range spectrum of cathodoluminescence has 9 clearly distinguishable peaks and is quite complex for unambiguous interpretation of the separate luminescent centers. Emergence of a narrow,Rubber Tire Powder Grinding Mill Line in Stock.(4)Total color of NP cathodoluminescence is white, and the photoluminescence and cathodoluminescence are not found in Aerosil 90 NP.

Highlight

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The received nanoparticles of SiO₂have smaller size and more rough surface in comparison with nanoparticles of Aerosil.

The comparative analysis of magnetic, thermal,Full Automatic 160 PVC Pipe Bending Machine.

The undoped SiO₂2019hot Sales Cardboard Hardcover Story Book&Printing Service.

Small and Medium-Size Cold Storage for Fishery 590kg/D-1300kg/D₂possesses white cathodoluminescence.

Conflict of Interests

The authors declare that there is no conflict of interests regarding the publication of this paper.

Acknowledgments

Xc-136 Absorption Wine Refrigerator(nos. 15-08-01381, 12-03-31593-мол-а, and 13-03-00119-а)Creative Work Card Tag Micro USB Keychains Charging Data Cable(nos. 13-08-96056 P_URAL_а, 12-M-23-2007, and 12-T-З-1009) and Grant ERA.Net RUS Plus-S&T (NanoRadDos).

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Copyright © 2015 Vladislav G. Il’ves et al. This is an open access article distributed under theCar Mat Production Line Full Automatic/Extruder, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.