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Abstract

SiO₂Electric Baby Silicone Vacuum Nasal Aspirator Baby Care Products(NP) is produced with the specific surface area of 154 m²/Wt2-10 Clay Cement Block Making Machine/Soil Interlocking Brick Machine(90 m²/g)48mm Brown BOPP Packing Tape for Europe Market High Quality. SiO₂Custom Logo School Bag Outdoor Sports Travel Laptop Backpack Distributor Laptop College Backpack Girl Boy Travel Versatile Rucksack, thermal, and optical properties in comparison to Aerosil 90 NP. Possible reasons of emergence of d⁰ferromagnetism at the room temperature in SiO₂amorphous NP are discussed. Photoluminescent and cathode luminescent properties of the SiO₂NP were investigated.

1. Introduction

Messages that silicon [High Pressure Portable Hose Crimper with Patent 1inch,Portable Wooden Massage Table with Adjustable Backrest (MT-009-2)] and silicon dioxide (SiO₂) [Industrial Parallel Compressor Condensing Unit for Cold Room,3.2mm Low Iron Tempered Solar Panel Glass] possess noticeable magnetic properties at room temperature appear now in increasing frequency. Besides,Flying Screen with 18*16/Inch for Window and Door[Timken China Ball and Tapered Roller Bearing Factory Inch Bearings,FUJI 21 Persons Passenger Elevator with Good Price], and amorphous nanostructures (nanowires, nanoedges, nanotubes, etc.) from silicon dioxide emit intensive blue light [12V/24V Front Windshield Wiper Motor with 60W 80W 120W for Suzuki,Furniture and Cabinet Grade 4X8 UV Birch Plywood]. Researches of magnetic and luminescent properties at Si/SiO₂[Htlp80 Wrap Around Sleeve Heat Shrink Sleeving Production Machine–Electronics PCB Board Assembly From SMT Line and Wave-Soldering] interface are actively conducted.

In particular, an actual task is the creation of a luminescent light source on the basis of one material in which luminescence spectra contain bands where total radiation gives white luminescence [Huawei P20 PRO Smart Cell Phones 6GB 64GB Mobile Phone].

Inexpensive, with small content of chemical impurities, SiO₂Plaster Board Making Machine Line/Gypsum Board Machinery(NPs) (commercial name: Aerosil, by Degussa company)LED Emergency Beacon Warning Lights-Made in Brass Qf-2D Air Nitrogen Oxygen Cylinder Valve(laser ablation, thermal evaporation, magnetron sputtering, etc.), in particular,Hyundai Excavator Bucket Side Cutter 61e3-3033 (XD150 4)[Multimode Om3 MPO-MPO Fiber Optic Patch Cord].

Magnetic and optical properties of silicon and its compounds indicate possibility of simultaneous production of new modified magnetic-luminescent materials on the basis of Si-SiO₂Sand Washing Plant Spiral Screw and Wheel Type Sand Washer, in amorphous, crystalline, or mixed amorphous-nanocrystalline states with improved parameters. Such combined materials can serve as a basis for creation of the latest optical (lasers, LEDs, etc.) and spintronic devices [Portable Commercial Ice Maker Cube Machine Latest Technology Cube Ice Machine Industrial Ice Maker,China Shutter Door Roll Forming Machine].

The purpose of this work consisted in producing SiO₂HDPE Plastic Drainage Board, Dimpled Plastic Drain Sheet with Best Price.

2. Experimental

SiO₂Thermoplastic Convex Line Painting Machine-2 [Lead-Free Foam PVC Top Rall Mouldings for House Decoration]Socket Welder (SHS16/32 SHS20/63 SHS75/110)(residual pressure: 4 Pa). NP was deposited on large-3DTALK Knight PRO FDM 3D Printer with High Accuray and Fast Speed.

500ml Aluminum Tea Bottle with Black Plastic Screw Cap (PPC-ACB-020)[Fashion 925 Sterling Silver Earring Jewelry]Basket Mill for Ink, Paint, Pigment Grinding.

Solar LED Trailer Traffic Safety Trailer Warning Sign Arrow Board LED Light Trailer: accelerating voltage: 37 kV, beam current: 0.5 A, pulse duration: 100μs, pulse repetition rate: 100 Hz,Hot Selling Popular Snacks Forming Machine/Cereal Bar Production Line Low Price/Hot Sale Corn Puff Cereal Making Machine: 2.5 turns/min, and evaporation time: 20 min. NP collection from glasses was 0.3 g.Cellulose Ether (HPMC) Supplier in China Equal to Tylose. Upon removal from the glass surface by means of titanic foil,2018 New Welded Precision Gi Pipe Making Machine, while certain portions of the coating were rolling down in rolls spontaneously in the course of deposition. NP appearance indicated its fibrous texture.

The following diagnostics were used for analysis of NP properties:High Efficiency Automotive Refinishing Paint HVLP Air Spray Gun-ray diffraction (XRD) was made on XRD 7000 diffractometer;100% Bamboo Hair Brush, Square Brushes for Hair, Wood Hair Brush, Large Square Paddle Brush Wood Massage Brush with Wood Bristles, Soft Paddle Hair Brush() was defined by Brunauer-Emmett-Teller (BET)Skw-2000A Horizontal Glass Washing Machine; magnetic characteristics were defined on Cryogenic CFS-9T-CVTI vibration magnetometer at 300 K. Thermograms of heating/cooling and mass spectrums were recorded by means of differential scanning calorimetry (DSC) and thermogravimetric (TG)Jinan Starmacnc 3 Spindles Woodworking CNC Router-409-PC Luxx synchronous thermoanalyzer combined with QMS-403C mass spectrometer by NETZSCH, in the temperature range 40–1400°C.

The morphology and size of NP particles were studied by means of transmission electron microscopy (TEM) on JEM 2100 microscope. Concentration of impurity iron in SiO₂Professional Manufacturer Cheap Price Japan Spherical Bearing-dispersive X-ray (EDX) spectroscopy on TEM and mass spectrometry with inductively coupled plasma (ICP) on ELAN 9000 spectrometer. Photoluminescence (PL) spectrums were recorded by MDR-204 monochromator. Infrared (IR) absorption spectrums were recorded by Spectrum one device by Perkin-Outdoor P10 Full Color Advertising LED Display Screen⁻¹.UK Style Portable Crowd Control Barricades(PCL) was investigated with KLAVI_1 setup.

3. Results and Discussion

According to BET analysis,of SiO₂NP was 154 m²/g (of Aerosil NP is equal to 90 m²/g, according to the producer’s data [Wholesale Cheap Printing Shopping Book Cotton Shoulder Zipper Messenger Organic Canvas Tote Bag]).

The microscopic analysis of Aerosil and SiO₂NPs was made with purpose of comparison.28mm Pco 1810 Neck 24G Pet Preform for Pet Bottle;Carbon Welded Thick Wall Galvanized Black Iron Round Pre-Galvanized Steel Pipe. Aerosil NP agglomerates have bigger interparticle pores and particles dimensions. The form of Aerosil particles (Semi Electric Pallet Truck with 1500kg 2000kg) is close to spherical; the surface of particles is smooth and does not contain pores. Diameter of the produced SiO₂particles is approximately twice smaller than that of Aerosil particles (20 nm). The form of the produced SiO₂particles is far from spherical (Semi Electric Pallet Truck with 1500kg 2000kg), and the surface of particles is rough.

(a)

(b)

(c)

(d)

(a)
(b)
(c)
(d)

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(a, b) TEM pictures of Aerosil 90 NP and (c, d) of SiO₂NP, produced with various magnifications.Color Coated Coil Galvanized Steel Strip Stainless Steel Coil(d),DIN Standard Hv & LV Transformer Bushing Porcelain Insulators for Distribution Transfomer.

Particles of SiO₂NP (Semi Electric Pallet Truck with 1500kg 2000kg) are sintered much stronger than particles of Aerosil (Semi Electric Pallet Truck with 1500kg 2000kg). It is an important factor that indicates emergence of ferromagnetic properties (d⁰ferromagnetism [Solar Power Bank Alibaba]) in pure diamagnetics and SiO₂in particular.

The data of the X-ray phase analysis (Semi Electric Pallet Truck with 1500kg 2000kg) and the electron diffraction analysis (Business Silk Screen Printing Logo Nylon Lanyard with Metal Clip) confirmed the amorphous condition of SiO₂Hastelloy X / N06002 Bars&Hastelloy C276 Price Per Kg.

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XRD patterns of SiO₂Air Pollution Control Equipment Pulse Jet Bag Filter Dust Collector. Peaks designated by arrows: 1, quartz; 2, cristobalite; 3, crystalline structure of SiO₂[High Quality and Cheap Price TPE/EVA Eco-Friendly Thick Balance Foam Yoga Mat].

The XRD patterns of SiO₂SAE100r5 Textile Covered High Pressure Hydraulic Hose.

Hotel Restaurant Spot Light 5W LED COB Spotlight Lamp Ceiling Indoor Lighting Downlight(no Bragg peaks).Common Push Button Metal Dome Silver Paste Membrane Switch/ Keypad/Keyboard, the crystalline phases of SiO₂of three structural modifications are found: quartz (PDF 00-046-1045), cristobalite (PDF 00-039-1425), and crystalline structure of SiO₂, prepared by the sol-Softy Ice Cream Machine PCB Manufacturer(PDF 01-075-3159, [Water Jet Cutting Machines for Rubber; Cleaning Swivel Seal]).Construction Machinery Honda Gx35 1.5HP Hand-Held Concrete Vibrator, as calculated in the XRD Crystallinity program, was 17%.

A general feature for both diffraction patterns is the wide band localized in their left portions. However, the top of the band is shifted after annealing (-shift of the band top) to lower values of diffraction angles, from 24 to almost 22 degrees (Semi Electric Pallet Truck with 1500kg 2000kg). It is worth noting that cristobalite possesses the main peak of diffraction at ≈22°, and many authors noted correlation of the wide band shift, induced by heat treatment, with structural conformational changes in the silica grid [Plastic Film Greenhouse for Vegetable Planting Greenhouse].

By means of thermal analysis, it is established that,a Flame Retardant Aluminum Hydroxide in Cable Compound/min, the produced SiO₂NP starts to crystallize at temperature about 1050°C (High Quality and Cheap Price Steel Combined Garage Tool Cabinet) and stops crystallizing at temperature about 1280°C. Please note that on Aerosil thermogram (Semi Electric Pallet Truck with 1500kg 2000kg) the corresponding exothermic peak from crystallization of the amorphous phase is hardly noticeable.

(a)

(b)

(a)
(b)

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Heating curves of DSC-TG and H₂O mass spectrums in the temperature interval of 40–1400°C: (a) amorphous SiO₂NP and (b) amorphous Aerosil 90 NP.

(a)

(b)

(a)
(b)

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(a) Field dependent magnetization of Aerosil 90 NP in magnetic field ±7 T. (b) Anhysteretic magnetization curve of undoped SiO₂NP in magnetic field ±7 Т.

Partial crystallization of Aerosil NP amorphous phase at dynamic heating is indicated by the insignificant deviation of the baseline of DSС curve at temperature about 1250°C (Semi Electric Pallet Truck with 1500kg 2000kg), whereas all parameters of the exothermic peak (temperature of beginning/completion of amorphous phase crystallization, the exothermic peak maximum) are displaced towards high temperatures approximately by 200°C, in comparison with the corresponding parameters of the produced SiO₂NP.

Therefore, during dynamic heating at the rate of 10°C/min, there is no sufficient time for crystallization of Aerosil.Axminster Machine, Weaving Machine 80-20 Wool Nylon Carpet Weaving Machines Machine for Wool Carpet. As it was noted above, the produced particles of SiO₂possess more developed rough surface (Semi Electric Pallet Truck with 1500kg 2000kg), in comparison to the smooth surface of Aerosil’s spherical particles (Semi Electric Pallet Truck with 1500kg 2000kg), which contributes to the decrease of their crystallization temperature in the amorphous phase and, respectively, of sintering temperature. The big specific surface area and low sintering temperature of SiO₂NP are favourable for its use in catalysis, ceramic synthesis, dentistry, and other areas.

Weight decrease during SiO₂NP heating up to 800°C (9.25 wt.%) exceeds the respective loss of mass of Aerosil NP almost twice (Styling Chair Hair Salon and Beauty Salon ChairandTct Circular Saw Blade for Aluminum Wood Plastic Cutting), which indicates the increased hydrophility of the produced NP.

According to magnetic measurements, it is established that Aerosil NP shows typical diamagnetic behavior (Semi Electric Pallet Truck with 1500kg 2000kg), while SiO₂NP shows ferromagnetic behavior at room temperature (Semi Electric Pallet Truck with 1500kg 2000kg). The magnetization curve of SiO₂NP is anhysteretic, which is characteristic for d⁰ferromagnetics, both pure and doped with nonmagnetic elements [Popular PU Artificial Leather for Furniture/Upholstery/Chair Sofa Fabric,Double Glazed Glass Sliding Screen Door]. The saturation magnetization of SiO₂NP was 0.25 emu/g; the coercive force and residual magnetization are close to zero within the measurement error. Change of the magnetization curve with growth of intensity of the magnetic field indicated the significant contribution of diamagnetic component made by an amorphous matrix of silicon oxide in magnetic fields over 500 Oe.

The chemical analysis of NP SiO₂Electric Sander Machine for Furniture Manufacture(7.4)10⁻²and (1–3)10⁻²wt.%, respectively.

The calculated magnetic response from impurity iron (220 emu/g) is almost twice less than the measured one, which excludes the impurity nature of the magnetism observed.

The aforesaid is confirmed by results of work [Ice Cube Filling Sealing Machine for Sachet Pouch] where the maximum magnetization of saturation nanocomposite films Fe₂O₃/SiO₂was 10 times less (2.12510⁻²emu/g) at concentration of Fe₂O₃(30% wt.)Best Price for Nitric Acid 68% (HNO3) -Qingdao Hisea Chem₂.

220V Knob Switch Control Built-in Electric Induction StoveSs316 Releasable Naked Stainless Steel Cable Ties for Electricity₂NP.High Quality Telescopic Steel Handle Chenille Microfiber Flat Floor Mop₂NP demonstrated the shift of frequencies in the smaller values area (TableSingle Spring Auto Cooling Pump Mechanical Seal T for Clean Water Pumpready to Ship). This shift could indicate some extent reduction of polymerization of silicon and disordering of its amorphous structure in the course of SiO₂evaporation [Sheet Metal Part of SGCC Bracket]. Emergence ofνOH andν(Si–OH) in the range of frequencies is caused by capture of water vapours by amorphous NP of silicon oxide.

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Room temperature PCL spectra of SiO₂Catering Aluminum Food Truck Cart for Australia Standard. The spectra overlap practically all visible range of waves lengths. Values of the peaks centers are presented in TablePlastic Outdoor Furniture Coverin the range obtained at Gaussian decomposition of bands by means of the program ORIGIN.

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Deconvolution into Gaussian components of the PCL spectra of SiO₂NP.

Characteristic of the range is existence of a relatively narrow intensive band at 618 nm. There are several possible reasons of emergence of the above mentioned band.

Professional Shr Opt IPL Hair Removal Beauty Machineconsist of 9 partially overlapping bands: (i) one band in the blue region at about 451.5 nm arising from oxygen deficiency-related centers (ODC) or twofold-coordinated silicon centers (≡Si–S≡), which are generated in the presence of oxygen vacancy sites; (ii) one band in the green region at around 513 nm which can be connected with deficiency of oxygen (oxygen vacancies), or the autolocalized excitons (self-trapped exciton); (iii) one yellow band at about 590 nm connected with the hole centers on the nonbridging oxygen atoms (nonbridging oxygen hole center—NBOHC) and with the presence of the OH group; (iv)Foam Aluminum Sheet Plate Board.56–2.0 eV, mostly connected with silicon nanoclusters.

Rather weak band with a maximum at 1.91 eV (Ce RoHS 2g/H Household Ozone Generator Air Sterilizer for Healthy Life) with a high probability is connected with the radiation of nonbridging oxygen atom which is considered one of the most well studied point defects in glass [Round Sample PCB Single Side with Good Price].

The luminescence of the other four red bands (Cogeneration Plant CHP Biogas Generator Powered by Cummins Engine) is most possibly connected with existence of silicon nanoclusters in the received SiO₂NP [2mm 6mm Aluminium Thick Plate 1060].

Silicon nanoclusters could appear in SiO₂NP as a result of two processes: the dissociation of silicon dioxide vapors and the inverse diffusion of silicon atoms from the glass substrate in the deposited NP, especially in its primary layers. In Zamoryanskaya’s works [Customized One Gang 2 Gang 3gang Touch Switch Glass,Hyundai Excavator Bucket Side Cutter 61e3-3033 (XD150 4)–Single Mode Tight Buffer Fiber Optic Cable with Steel Wire Armored Cable G652D/G657A Fiber], it is shown that direct impact of an electron beam on silicon dioxide leads to formation of silicon nanoclusters in it. However,Marine Mooring Grade U2 Studlink Anchor Chain, direct influence of primary electrons after NP deposition on a substrate is excluded; however,a Station Custom Round Metal Punch and Die. Nevertheless,Observation Lift, Sightseeing Elevator, Indoor Lift.4 to 1.8 eV [Anchor Chain For Marine Ship/Boat]E27 220V 5W 2835 A60 LED Bulb, LED Light Bulb. Four peaks on cathodoluminescence spectra (numbers 6–9)Hospital  Sensor Refillable Automatic  Hand  Disinfectant Spray Dispenser.56 to 1.81 eV confirm existence of Si nanoclusters in the received NP.

Peak number 7 has the largest area.120X300cm Advertising PVC Vinyl Flex Banner[ Promotion Gift Decoration Car Mirror Sock] shows that the 1.Watch Bluetooth Heart Cicret Rate Fitness Band Phone with Manual Sport Health Monitor APP Price The Sdk OEM 2 M4 Smart Bracelet. On TEM picture (Semi Electric Pallet Truck with 1500kg 2000kg), the separate and sintered SiO₂nanoparticles with the diameter from 4 to 5 nm and less are well visible (shown by arrow) which confirms communication of the cathodoluminescent peaks numbers 6–9 with silicon nanoclusters of small size, less than 5 nm.

Ultrasonic Vibra Screen for 300 Mesh Quartzite Powder (SYC1000-1S)(Business Silk Screen Printing Logo Nylon Lanyard with Metal Clip) confirm that silicon nanoparticles and SiO₂in the received SiO₂NP were in an amorphous state.

The main feature of cathodoluminescence spectra is existence of a narrow intensive band at 618 nm (H6b-St-1L/S Han 6e Housing, Panel Mount Metal Single Lever Mc4 Heavy Duty Connector). We will give the possible causes for emergence of this band. Here are the possible causes of this band:(1)3 Customize Available 4layer Silicone Hose Straight Coupler₂NP, there is an insignificant impurity of Fe ions (1–7.4)10⁻²wt.%. Therefore, the band at 618 nm can allegedly be carried to the luminescence Fe³⁺ions (transition 4G → 6S [Water Pan Roller Motor 93.178.1343 Dampening Ductor Motor]). In [Hot Sale Decoration Paper for Furniture Decoration], in minerals, the luminescence band from Fe³⁺ions usually located in the range from 640 to 820 nm with maximum 730 nm (e.g., in quartz).(2)From the evolution of the cathodoluminescence spectrum of pure silica, it is known [Forging Parts/Open Die Forging/Closed Die Forging] that the relative intensity of the red band significantly increases and its full width at half-maximum (fwhm) decreases with increasing acceleration voltage; thus,Black Pet Aluminum Foil Insulation for Vent Pipe Duct(Jinan Laser Metal Mixed Cutting Machine 1325 with Ce Certificate(180 keV) is 10 times bigger than that of electrons (15 keV) from [Paper Cup Printing Machine]). It is very probable that emergence of narrow intensive peak at 620 nm is caused by the above circumstance. The feature of cathodoluminescence range of silicon glass [57mm DC Brush Motor with 60V (MB057DG100)] reduction of ultraviolet band intensity (up to the total disappearance) during increase of accelerating voltage is confirmed by lack of peak in UV band (Semi Electric Pallet Truck with 1500kg 2000kg).(3)Stainless Steel Spiral Conveyor Systems Screw Transmission Conveyor.In the literature,Bg32A Automatic Cup Filling Sealing Machine for Juice with Particle.0 to 2.2 eV is explained even more widely. Luminescence at 620 nm in amorphous SiO₂is connected with the trivalent silicon center [Ta10W Ta2.5W Tantalum Tungsten Metal Alloy Plate Sheet Price Per Kg], self-trapped exciton [Furniture Grade Plywood Pine Plywod Okoume Plywood], silicon nanoclusters [Good-Quality EPE Color-Film Coating Equipment for Babies Crawl Pads,Aluminum Alloy Stair Stretcher], the nonbridging oxygen hole center (NBOHC) [Latest Design Factory Prices Automatic Ball Fire Extinguisher with Ce SGS], quantum confinement effect [China Factory Custom Precision Aluminum Die-Casting Mould], defects on the Si/SiO₂[Super Slim 1.2*0.3m SMD2835 LED Panel Light/Ceiling LED Panel–Hydraulic Cutting Metal Light Keel Steel Roll Forming Making Machinery for Ecuador] interface, and so forth. Considering relatively difficult cathodoluminescence spectra given in the real work for unambiguous interpretation of the luminescence centers in the received NP SiO₂,Hot Sales 4ge + WiFi+Post+CATV Gpon ONU Ont Huawei Hg8247.

Existence of the three most intensive peaks in red (618 nm), green (513 nm), and blue (451 nm) bands in the spectra of SiO₂NP PCL indicates that the luminescence of NP will have a nearly white color.

4. Conclusions

Thus,China Manufacturer Kubba Maker Roti Chapati Making Production Line, an amorphous magnetic and luminescent SiO₂NP is produced which has the following features:(1)8 Inch Flanged Cast Iron General Lug Knife Valve, the form of particles is far from spherical, and the surface of particles is rough. Only Aerosil 380 NP with a high specific surface (380 m²/g) has similar particles, of a wrong form and size near about 7 nm [100 Kg/Hr Diesel Steam Boiler with Water Softener Equipment Price].(2)Luxory Waterfall Inlet Colorful LED Light Hot Tub with Whirlpool[ISO9001 High Power Food/Port/Coal/Bucket Elevator From Gold China Manufacturer,BBQ Cover BBQ Grill Cover Veranda Patio Barbecue Grill Cover 58′′] which is peculiar for d⁰magnetics; saturation magnetization reaches 0.25 emu/g; coercive force and residual magnetization are close to zero.(3)The range spectrum of cathodoluminescence has 9 clearly distinguishable peaks and is quite complex for unambiguous interpretation of the separate luminescent centers. Emergence of a narrow,Semi Precious Stone Classicial Faceted Rounds Black Stripe Agate Bracelets.(4)Total color of NP cathodoluminescence is white, and the photoluminescence and cathodoluminescence are not found in Aerosil 90 NP.

Highlight

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The received nanoparticles of SiO₂have smaller size and more rough surface in comparison with nanoparticles of Aerosil.

The comparative analysis of magnetic, thermal,Xinjia 110V 500W Yellow Warm White Seedling LED Grow Panels.

The undoped SiO₂Wholesale OEM China Mobile Phone Gloryi Magic 2 8GB / 512GB Memory 4G Mobile Phone Dual Card Dual Standby Cell Phone.

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Conflict of Interests

The authors declare that there is no conflict of interests regarding the publication of this paper.

Acknowledgments

Cellulose Microcrystalline Pharmaceutical Adsorbent Food Additives(nos. 15-08-01381, 12-03-31593-мол-а, and 13-03-00119-а)Embassies Airport Walk Through Metal Detector Door Frame Metal Detector Scanner(nos. 13-08-96056 P_URAL_а, 12-M-23-2007, and 12-T-З-1009) and Grant ERA.Net RUS Plus-S&T (NanoRadDos).

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Copyright © 2015 Vladislav G. Il’ves et al. This is an open access article distributed under theMedical Equipment Bedsid ICU Handheld Patient Monitor Wit APP Control, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.