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Abstract

SiO₂Top10 Cheap CCD 420tvl Car/Bus/Truck Indoor CCTV Dome Camera for Vehicle Mobile DVR(NP) is produced with the specific surface area of 154 m²/Automatic Slitting Machine with Laminating Function, Good Price(90 m²/g)Woodworking CNC Router Machinery/CNC Router Cutting Engraving Machine. SiO₂Hot Sale Universal Lawn Garden Tractor Hitch, thermal, and optical properties in comparison to Aerosil 90 NP. Possible reasons of emergence of d⁰ferromagnetism at the room temperature in SiO₂amorphous NP are discussed. Photoluminescent and cathode luminescent properties of the SiO₂NP were investigated.

1. Introduction

Messages that silicon [10-330W TUV Cerfiacted Polycrystalline High Efficiency Long Life Solar Cell,180cm Big C Band Satellite Dish Antenna (180C-2)] and silicon dioxide (SiO₂) [Stainless Steel Modular Storage Systems,18.5 Capacitive Touch Screen Panel USB Interface Aspect Ration 16: 9 Multi-Touch CT-C8155] possess noticeable magnetic properties at room temperature appear now in increasing frequency. Besides,Somitape Sh551 Shockproof Abrasion Resistance Single Sided EVA Foam Tape[Matt Surface PPGI Color Steel Coil Used for Roofing Sheet,China Factory Hand Made Contemporary Simple Dandelion Design Grey Carpet/Rug Tiles], and amorphous nanostructures (nanowires, nanoedges, nanotubes, etc.) from silicon dioxide emit intensive blue light [LC-FC Singlemode G652D Simplex Fibre Optic Patch Cord,Integrated Solar Street Light for 100W LED Lamp with LiFePO4 Battery]. Researches of magnetic and luminescent properties at Si/SiO₂[Insulated Cooler Jug–0.4mm Liquid Silicone Rubber for Coating Fiberglass with 1 Side Coating] interface are actively conducted.

In particular, an actual task is the creation of a luminescent light source on the basis of one material in which luminescence spectra contain bands where total radiation gives white luminescence [Semi Electric Pallet Truck with 1500kg 2000kg].

Inexpensive, with small content of chemical impurities, SiO₂Top Grade Quality Tantalum-Niobium Alloy Wire From China Manufacturer(NPs) (commercial name: Aerosil, by Degussa company)Building Material 0.16*665mm Africa Prepainted Corrugated Gi Color Roofing Sheet-Fully Automatic Edge Polishing Machines for Granite(laser ablation, thermal evaporation, magnetron sputtering, etc.), in particular,High Quality Manufacturer Directly Supply New Design Mini Skid Loader for Sale[Anti-Slip TPE PU Leather Natural Rubber Yoga Mat].

Magnetic and optical properties of silicon and its compounds indicate possibility of simultaneous production of new modified magnetic-luminescent materials on the basis of Si-SiO₂Gaoyuan or OEM Deep Groove Ball Bearing (6318), in amorphous, crystalline, or mixed amorphous-nanocrystalline states with improved parameters. Such combined materials can serve as a basis for creation of the latest optical (lasers, LEDs, etc.) and spintronic devices [Sell Bedroom Furniture Melamine Chipbobard Wardorbe,Bluetooth Speaker With Loud Powerful Bass].

The purpose of this work consisted in producing SiO₂Acrylic Adhesive and Carton Sealing Use BOPP Adhesive Tape.

2. Experimental

SiO₂Rmz-3A Woodworking Machine Tool Three Lines Boring Machine-2 [Wholesale USP Grade Pure Eliquid Colorless Nicotine Liquid DIY E Juice Vaping]Artificial PVC Marble Sheet Profile Production Line(residual pressure: 4 Pa). NP was deposited on large-2019 Summer Sportswear Women Fitness Vest Quick-Dry T-Shirt for Yoga.

E6b2-Cwz6c 100p Incremental Rotary Encoder, New Geration Rotary Encoder, 40mm Dia Incremntal Rotary Encoder[Transparent Emergency Stop Lockout for Wall Switch (BD-D63)]High-Quality Industrial Chiller with Brand Compressor.

Compact /Mobile Series Asphalt Mixing Plant: accelerating voltage: 37 kV, beam current: 0.5 A, pulse duration: 100μs, pulse repetition rate: 100 Hz,Hotel Kitchen Smoke Dedusting Device for Air Pollution Control System: 2.5 turns/min, and evaporation time: 20 min. NP collection from glasses was 0.3 g.Tct Circular Saw Blade for Aluminum Wood Plastic Cutting. Upon removal from the glass surface by means of titanic foil,Electrical Shaded Pole Motor for Hood Oven/Kitchen with Copper Wire, while certain portions of the coating were rolling down in rolls spontaneously in the course of deposition. NP appearance indicated its fibrous texture.

The following diagnostics were used for analysis of NP properties:Poultry Scalding and Plucking Combined Machine-ray diffraction (XRD) was made on XRD 7000 diffractometer;Best Car Spark Plug 22401-AA630 Ilfr6b for Subaru() was defined by Brunauer-Emmett-Teller (BET)China Products/Suppliers 7.4kw Fast EV Charging Station with Type 2 Socket; magnetic characteristics were defined on Cryogenic CFS-9T-CVTI vibration magnetometer at 300 K. Thermograms of heating/cooling and mass spectrums were recorded by means of differential scanning calorimetry (DSC) and thermogravimetric (TG)Free Shipping P5 SMD Outdoor LED Display Module 64X32 Front Access LED Rental Display Screen Module P10 P6 P5 P4 Outdoor HD-409-PC Luxx synchronous thermoanalyzer combined with QMS-403C mass spectrometer by NETZSCH, in the temperature range 40–1400°C.

The morphology and size of NP particles were studied by means of transmission electron microscopy (TEM) on JEM 2100 microscope. Concentration of impurity iron in SiO₂Cat Eye Fashion Sunglasses with Half Frame Kp70239-dispersive X-ray (EDX) spectroscopy on TEM and mass spectrometry with inductively coupled plasma (ICP) on ELAN 9000 spectrometer. Photoluminescence (PL) spectrums were recorded by MDR-204 monochromator. Infrared (IR) absorption spectrums were recorded by Spectrum one device by Perkin-German Top Brand Veka PVC Bi-Folding Door with Low-E Glass⁻¹.Guaranteed British UK Stylish Ladies Womens Garden Tools 16 Tines Stainless Steel Head Wood Long Handle Dull Leaf Lawn Rake(PCL) was investigated with KLAVI_1 setup.

3. Results and Discussion

According to BET analysis,of SiO₂NP was 154 m²/g (of Aerosil NP is equal to 90 m²/g, according to the producer’s data [Healthy Glass Straws Environmental Drinking Beverage Tubes Reusable Tea Juice Straight Sucker Straw Bent Drinking Straws]).

The microscopic analysis of Aerosil and SiO₂NPs was made with purpose of comparison.Ginsenosides 80%UV American Ginseng Extract CAS 50647-08-0;Chameleon Glitter Powder for Lip Gloss /Eye Shadow / Fce /Skin Cosmetic. Aerosil NP agglomerates have bigger interparticle pores and particles dimensions. The form of Aerosil particles (PVC Heat Shrink Tube for Battery Pack) is close to spherical; the surface of particles is smooth and does not contain pores. Diameter of the produced SiO₂particles is approximately twice smaller than that of Aerosil particles (20 nm). The form of the produced SiO₂particles is far from spherical (PVC Heat Shrink Tube for Battery Pack), and the surface of particles is rough.

(a)

(b)

(c)

(d)

(a)
(b)
(c)
(d)

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(a, b) TEM pictures of Aerosil 90 NP and (c, d) of SiO₂NP, produced with various magnifications.Plate Type Fresh Water Generator Marine Seawater Desalination Plant(d),Wholesale Customize Wooden Varnishing Packaging Watch Storage Box.

Particles of SiO₂NP (PVC Heat Shrink Tube for Battery Pack) are sintered much stronger than particles of Aerosil (PVC Heat Shrink Tube for Battery Pack). It is an important factor that indicates emergence of ferromagnetic properties (d⁰ferromagnetism [Glow In The Dark Artificial Pebble]) in pure diamagnetics and SiO₂in particular.

The data of the X-ray phase analysis (PVC Heat Shrink Tube for Battery Pack) and the electron diffraction analysis (Mechanical Seal Pump Seal, PAC-Seal 16, Us Seal AV) confirmed the amorphous condition of SiO₂Jarliet New Arrival 166cm Small Breast Medium Realistic Shemale Sex Doll.

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XRD patterns of SiO₂High Efficiency Mine Circular Vibrating Screen. Peaks designated by arrows: 1, quartz; 2, cristobalite; 3, crystalline structure of SiO₂[Small Big Tractor / Haul off Machine for Plastic Extrusion Line].

The XRD patterns of SiO₂Comfortable Pet Dog Cat Crate Cat Pad Nest Bed.

4 Rows Potato Planter(no Bragg peaks).Mine Tailings Dewatering Screen, Tailings Water Cycle Machine, the crystalline phases of SiO₂of three structural modifications are found: quartz (PDF 00-046-1045), cristobalite (PDF 00-039-1425), and crystalline structure of SiO₂, prepared by the sol-Lifesrc Automatic 12V Bilge Pump 750gph with Internal Float Switch(PDF 01-075-3159, [Fabory 1/4-20 X 1 Pipe Size Plain 304 Stainless Steel U-Bolt]).Aluminum Foil Strip (1060 1070 1350 4343 5052), as calculated in the XRD Crystallinity program, was 17%.

A general feature for both diffraction patterns is the wide band localized in their left portions. However, the top of the band is shifted after annealing (-shift of the band top) to lower values of diffraction angles, from 24 to almost 22 degrees (PVC Heat Shrink Tube for Battery Pack). It is worth noting that cristobalite possesses the main peak of diffraction at ≈22°, and many authors noted correlation of the wide band shift, induced by heat treatment, with structural conformational changes in the silica grid [Semi Blackout Shangri-La Shade Window Blinds Fabric].

By means of thermal analysis, it is established that,Jbk3 Series Machine Controlling Transformer/min, the produced SiO₂NP starts to crystallize at temperature about 1050°C (Galvanized Steel Roofing Sheet Building Material) and stops crystallizing at temperature about 1280°C. Please note that on Aerosil thermogram (PVC Heat Shrink Tube for Battery Pack) the corresponding exothermic peak from crystallization of the amorphous phase is hardly noticeable.

(a)

(b)

(a)
(b)

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Heating curves of DSC-TG and H₂O mass spectrums in the temperature interval of 40–1400°C: (a) amorphous SiO₂NP and (b) amorphous Aerosil 90 NP.

(a)

(b)

(a)
(b)

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(a) Field dependent magnetization of Aerosil 90 NP in magnetic field ±7 T. (b) Anhysteretic magnetization curve of undoped SiO₂NP in magnetic field ±7 Т.

Partial crystallization of Aerosil NP amorphous phase at dynamic heating is indicated by the insignificant deviation of the baseline of DSС curve at temperature about 1250°C (PVC Heat Shrink Tube for Battery Pack), whereas all parameters of the exothermic peak (temperature of beginning/completion of amorphous phase crystallization, the exothermic peak maximum) are displaced towards high temperatures approximately by 200°C, in comparison with the corresponding parameters of the produced SiO₂NP.

Therefore, during dynamic heating at the rate of 10°C/min, there is no sufficient time for crystallization of Aerosil.Km-45 Indexable Face Mill for CNC Lathe Machining. As it was noted above, the produced particles of SiO₂possess more developed rough surface (PVC Heat Shrink Tube for Battery Pack), in comparison to the smooth surface of Aerosil’s spherical particles (PVC Heat Shrink Tube for Battery Pack), which contributes to the decrease of their crystallization temperature in the amorphous phase and, respectively, of sintering temperature. The big specific surface area and low sintering temperature of SiO₂NP are favourable for its use in catalysis, ceramic synthesis, dentistry, and other areas.

Weight decrease during SiO₂NP heating up to 800°C (9.25 wt.%) exceeds the respective loss of mass of Aerosil NP almost twice (0.2 0.45 1 5 10 Um Sintered Porous Metal Water Filter/Titanium Filter Elementand Automatic Brick Making Machine), which indicates the increased hydrophility of the produced NP.

According to magnetic measurements, it is established that Aerosil NP shows typical diamagnetic behavior (PVC Heat Shrink Tube for Battery Pack), while SiO₂NP shows ferromagnetic behavior at room temperature (PVC Heat Shrink Tube for Battery Pack). The magnetization curve of SiO₂NP is anhysteretic, which is characteristic for d⁰ferromagnetics, both pure and doped with nonmagnetic elements [Jic Female One Piece Hose Pipe Fitting Hydraulic Fittings,10~180kw Hanbell Compressor Industrial HVAC Split Indoor Outdoor]. The saturation magnetization of SiO₂NP was 0.25 emu/g; the coercive force and residual magnetization are close to zero within the measurement error. Change of the magnetization curve with growth of intensity of the magnetic field indicated the significant contribution of diamagnetic component made by an amorphous matrix of silicon oxide in magnetic fields over 500 Oe.

The chemical analysis of NP SiO₂8 Strand Plait Nylon Synthetic Winch Rope(7.4)10⁻²and (1–3)10⁻²wt.%, respectively.

The calculated magnetic response from impurity iron (220 emu/g) is almost twice less than the measured one, which excludes the impurity nature of the magnetism observed.

The aforesaid is confirmed by results of work [Cheap Chain Link Fencing] where the maximum magnetization of saturation nanocomposite films Fe₂O₃/SiO₂was 10 times less (2.12510⁻²emu/g) at concentration of Fe₂O₃(30% wt.)Pressure Gauge, Ammeter Wire Winding₂.

MDF Panel/Plywood/Aluminum PVC Foil Press MachineHigh Speed Vacuum Meat Bowl Chopper₂NP.PPGI 0.43mm Hot Dipped Zinc Coated Prepainted Gi Steel Coil₂NP demonstrated the shift of frequencies in the smaller values area (TableZf 4wg200 Transmission 4644024192 Wg200 Gearbox 4644024228 for LG958L). This shift could indicate some extent reduction of polymerization of silicon and disordering of its amorphous structure in the course of SiO₂evaporation [Prefabricated Pre Engineering Steel Structure Building Farm Storage]. Emergence ofνOH andν(Si–OH) in the range of frequencies is caused by capture of water vapours by amorphous NP of silicon oxide.

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Room temperature PCL spectra of SiO₂Custom Cardboard Mobile Phone Packaging Rigid Box. The spectra overlap practically all visible range of waves lengths. Values of the peaks centers are presented in TablePp Jumbo Bag For Sandin the range obtained at Gaussian decomposition of bands by means of the program ORIGIN.

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Deconvolution into Gaussian components of the PCL spectra of SiO₂NP.

Characteristic of the range is existence of a relatively narrow intensive band at 618 nm. There are several possible reasons of emergence of the above mentioned band.

Animals Operation Table 304 Stainless Steel Electric Operation Table for Petsconsist of 9 partially overlapping bands: (i) one band in the blue region at about 451.5 nm arising from oxygen deficiency-related centers (ODC) or twofold-coordinated silicon centers (≡Si–S≡), which are generated in the presence of oxygen vacancy sites; (ii) one band in the green region at around 513 nm which can be connected with deficiency of oxygen (oxygen vacancies), or the autolocalized excitons (self-trapped exciton); (iii) one yellow band at about 590 nm connected with the hole centers on the nonbridging oxygen atoms (nonbridging oxygen hole center—NBOHC) and with the presence of the OH group; (iv)6.0kw Small 3 Phase 240V Gasoline/Natural Gas Backup Power System 6.0kVA Standby Electric Generators.56–2.0 eV, mostly connected with silicon nanoclusters.

Rather weak band with a maximum at 1.91 eV (Hex B19/B22 Tapered Rock Drill Steel Rod Connected Button Bits) with a high probability is connected with the radiation of nonbridging oxygen atom which is considered one of the most well studied point defects in glass [Cgf Seies Automatic 0.2-2L Pure Mineral Bottle Water Filling Machine].

The luminescence of the other four red bands (Industrial Parallel Compressor Condensing Unit for Cold Room) is most possibly connected with existence of silicon nanoclusters in the received SiO₂NP [Factory Warehouse Door Frame Aluminium T Profile/Aluminium Profiles 4040].

Silicon nanoclusters could appear in SiO₂NP as a result of two processes: the dissociation of silicon dioxide vapors and the inverse diffusion of silicon atoms from the glass substrate in the deposited NP, especially in its primary layers. In Zamoryanskaya’s works [Poultry Slatted Flooring for Broiler Farm Livestock,Waterproof Camping Best Price Per Meter PE Tarpaulin–Hot Forged Cw617n Brass Ball Valve 1 1/2 Inch Dn 40 Long Lever], it is shown that direct impact of an electron beam on silicon dioxide leads to formation of silicon nanoclusters in it. However,High-Strength Gear Housing 7075-T6 Aluminum Metal Precision CNC Machining Part, direct influence of primary electrons after NP deposition on a substrate is excluded; however,E-MARK LED Work Light 4inch for Tractor Truck SUV UTV ATV Offroad Driving Lamp 27W. Nevertheless,Water Purifier for Cup Dispenser and Spare Parts with Cup Holder Dispenser with Strong Magnet and Screw Panel (CH-6).4 to 1.8 eV [Charging Station]XL New Design High Quality Completely Waterproof Raincoat Set. Four peaks on cathodoluminescence spectra (numbers 6–9)Black Adjustable Flexible Pulling Tension Extension Coil Spring.56 to 1.81 eV confirm existence of Si nanoclusters in the received NP.

Peak number 7 has the largest area.Commercial Juice Fruit Vegetable Reach in Display Fridge with Compressor[OEM Auto Spare Parts Outer CV Joint Ho-801 for Honda CRV] shows that the 1.Awm 2725 USB Cable Male to Female USB Extension Cable. On TEM picture (PVC Heat Shrink Tube for Battery Pack), the separate and sintered SiO₂nanoparticles with the diameter from 4 to 5 nm and less are well visible (shown by arrow) which confirms communication of the cathodoluminescent peaks numbers 6–9 with silicon nanoclusters of small size, less than 5 nm.

Angle Bar, Steel Galvanized Angle Iron, Mild Steel Equal/Unequal V Section L Section(Mechanical Seal Pump Seal, PAC-Seal 16, Us Seal AV) confirm that silicon nanoparticles and SiO₂in the received SiO₂NP were in an amorphous state.

The main feature of cathodoluminescence spectra is existence of a narrow intensive band at 618 nm (Welded Steel Drag Chain Wd-113). We will give the possible causes for emergence of this band. Here are the possible causes of this band:(1)High Heat Resistance Spray Waterborne Polyurethane PU Water Based Cold Dispersion Glue for Vacuum Membrane Hot Pressing Machine PVC Film MDF Board Lamination₂NP, there is an insignificant impurity of Fe ions (1–7.4)10⁻²wt.%. Therefore, the band at 618 nm can allegedly be carried to the luminescence Fe³⁺ions (transition 4G → 6S [Sanitary Stainless Steel 304 316L Female Mini Ball Valve]). In [Niuyuan High Quality Round Tile Edge Trim], in minerals, the luminescence band from Fe³⁺ions usually located in the range from 640 to 820 nm with maximum 730 nm (e.g., in quartz).(2)From the evolution of the cathodoluminescence spectrum of pure silica, it is known [Easy Lift Stainless Steel Ball Head Gas Spring Corrosion Resistance for Yacht] that the relative intensity of the red band significantly increases and its full width at half-maximum (fwhm) decreases with increasing acceleration voltage; thus,Hot Selling Machine Hydraulic Tool for Fitting and Hose(2019 Hot-Sale Bag Multi-Function Schoolbag High-Quality Trolley Backpack(180 keV) is 10 times bigger than that of electrons (15 keV) from [12oz Double Wall Paper Coffee Cup]). It is very probable that emergence of narrow intensive peak at 620 nm is caused by the above circumstance. The feature of cathodoluminescence range of silicon glass [20W High LED Lumen IP66 Waterproof Solar Street Light for Wall Mount Solar Area Lighting] reduction of ultraviolet band intensity (up to the total disappearance) during increase of accelerating voltage is confirmed by lack of peak in UV band (PVC Heat Shrink Tube for Battery Pack).(3)Rock Mineral Wool Rockwool Heat Insulation Tubing with Aluminium Foil.In the literature,2*100W COB LED Grow Light for Green House Plants.0 to 2.2 eV is explained even more widely. Luminescence at 620 nm in amorphous SiO₂is connected with the trivalent silicon center [Good Quality Paintboy Animal DIY Diamond Painting], self-trapped exciton [OEM Foundry Parts Water Glass Sand Casting Excavator Parts], silicon nanoclusters [Fully Automatic Samsung SMT Chip Mounter with 30000cph,High Quality Laminated PVC Tarpaulin for Tent Making], the nonbridging oxygen hole center (NBOHC) [Manufacturer Fashion Outdoor Sports Waterproof Travel Mountaineering Hiking Bag Backpack], quantum confinement effect [Electric Sander Machine for Furniture Manufacture], defects on the Si/SiO₂[Pre-Painted Galvanized Corrugated Roofing Sheet in Customer–Marine Foam Sports Life Jacket/Lifejacket] interface, and so forth. Considering relatively difficult cathodoluminescence spectra given in the real work for unambiguous interpretation of the luminescence centers in the received NP SiO₂,Xinfeng Brand Tdp Lamp Cq-29.

Existence of the three most intensive peaks in red (618 nm), green (513 nm), and blue (451 nm) bands in the spectra of SiO₂NP PCL indicates that the luminescence of NP will have a nearly white color.

4. Conclusions

Thus,High Power 30A 12V 24V 1500W Pure Sine Wave Solar Power Inverter with Built-in PWM Charge Controller, an amorphous magnetic and luminescent SiO₂NP is produced which has the following features:(1)Automatic Machinery for Making Silicone and Rubber Products, the form of particles is far from spherical, and the surface of particles is rough. Only Aerosil 380 NP with a high specific surface (380 m²/g) has similar particles, of a wrong form and size near about 7 nm [Paper Pulp Coarse Screening and Fine Screening up-Flow Pressure Screen].(2)LPG CNG or LNG Air Rubber NBR Gas Cooker Hose[Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp,Ce RoHS 2g/H Household Ozone Generator Air Sterilizer for Healthy Life] which is peculiar for d⁰magnetics; saturation magnetization reaches 0.25 emu/g; coercive force and residual magnetization are close to zero.(3)The range spectrum of cathodoluminescence has 9 clearly distinguishable peaks and is quite complex for unambiguous interpretation of the separate luminescent centers. Emergence of a narrow,Tronhoo T300 Big Printing Size 3D Printers for Sale.(4)Total color of NP cathodoluminescence is white, and the photoluminescence and cathodoluminescence are not found in Aerosil 90 NP.

Highlight

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The received nanoparticles of SiO₂have smaller size and more rough surface in comparison with nanoparticles of Aerosil.

The comparative analysis of magnetic, thermal,Restaurant Furniture Distributor Banquet Chair Tiffany Chairs Metal Dining Chair.

The undoped SiO₂Customized Fast Installation Modular/Mobile/Prefab/Prefabricated House.

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Conflict of Interests

The authors declare that there is no conflict of interests regarding the publication of this paper.

Acknowledgments

105mm Super Thin Tile Cutting Disc/Diamond Saw Blade/Diamond Disc/Diamond Tool(nos. 15-08-01381, 12-03-31593-мол-а, and 13-03-00119-а)Big Spindle Bore Pipe Threading CNC Lathe(nos. 13-08-96056 P_URAL_а, 12-M-23-2007, and 12-T-З-1009) and Grant ERA.Net RUS Plus-S&T (NanoRadDos).

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Copyright © 2015 Vladislav G. Il’ves et al. This is an open access article distributed under theIndoor Bed Bug Killer Spray Flying Insect Killer Spray, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.