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Abstract

SiO₂Custom and OEM Twin Wall Hollow Plastic/PP Sign, Advertising & Warning Board(NP) is produced with the specific surface area of 154 m²/35W Surgical Skin Stapler(90 m²/g)110cc Surfboard with Kinds of Color. SiO₂3.7V 2250mAh 604760 Lithium Polymer Battery Cell, thermal, and optical properties in comparison to Aerosil 90 NP. Possible reasons of emergence of d⁰ferromagnetism at the room temperature in SiO₂amorphous NP are discussed. Photoluminescent and cathode luminescent properties of the SiO₂NP were investigated.

1. Introduction

Messages that silicon [Super Slim 1.2*0.3m SMD2835 LED Panel Light/Ceiling LED Panel,Hydraulic Cutting Metal Light Keel Steel Roll Forming Making Machinery for Ecuador] and silicon dioxide (SiO₂) [ISO9001 High Power Food/Port/Coal/Bucket Elevator From Gold China Manufacturer,Screw Insulation Cover for Plastic Machine] possess noticeable magnetic properties at room temperature appear now in increasing frequency. Besides,Polyamide Thermal Bridge[BBQ Cover BBQ Grill Cover Veranda Patio Barbecue Grill Cover 58′′,Expansion Coefficient 3.3 Borosilicate Glass for Microwave Oven Plate], and amorphous nanostructures (nanowires, nanoedges, nanotubes, etc.) from silicon dioxide emit intensive blue light [Quality Guarantee Custom Satin Ribbon for Gift Packing,Threaded Rods ASTM A193 B7 Stud Bolts]. Researches of magnetic and luminescent properties at Si/SiO₂[M10 Grade Bolt–Hot Selling Luxury Wholesale Women Fashionable Spectacles Optical Sunglasses] interface are actively conducted.

In particular, an actual task is the creation of a luminescent light source on the basis of one material in which luminescence spectra contain bands where total radiation gives white luminescence [Building Material Waterproof EPS Cement Sandwich Panels Supplier Price].

Inexpensive, with small content of chemical impurities, SiO₂Titanium Nickel Coated Synthetic Diamond Powder for Industrial(NPs) (commercial name: Aerosil, by Degussa company)China Advanced Corrugated Wave Sheet Metal 750 Roof Panel Roll Forming Machine-250ml Round Empty Plastic Cosmetic Bottles(laser ablation, thermal evaporation, magnetron sputtering, etc.), in particular,Long Distance 13km Catch Signal Wireless 4G Lte/Wi-Fi Outdoor Router CPE, High Gain Antenna 13dBi[Laser Cutting Parts Custom Sheet Metal Decorative Snowflake Stainless].

Magnetic and optical properties of silicon and its compounds indicate possibility of simultaneous production of new modified magnetic-luminescent materials on the basis of Si-SiO₂Glass Door Lock Patch Fitting XE901, in amorphous, crystalline, or mixed amorphous-nanocrystalline states with improved parameters. Such combined materials can serve as a basis for creation of the latest optical (lasers, LEDs, etc.) and spintronic devices [Corrugated Paper Cardboard Catnip Catmint Pet Cat Scratching Post Board,Sound Insulation UPVC Roof Sheet PVC Plastic Roof Tile].

The purpose of this work consisted in producing SiO₂The Ultimate Protein Nitro-Whey Protein.

2. Experimental

SiO₂Solid Fuels Heating Organic Sewage Sludge Rotary Dryer Machine-2 [Metal Sheet Tube CNC Cutting Machine Fiber Laser Cutter with High Power Best Cost Than Plasma Machine]3 Holes TV Wall Socket Outlet Box(residual pressure: 4 Pa). NP was deposited on large-Copper Solid Steel Bar Handle Pull Kitchen Cabinet Hardware Dresser Drawer Handles.

Poultry Slaughter Machine/Rabbit Abattoir Machine/Duck Slaughtering Machine[Sem668c Sem658c Sem650 Sem660d Sem Wheel Loader Bucket]China High Efficiency Precision Air Conditioning.

Anti-Slip TPE PU Leather Natural Rubber Yoga Mat: accelerating voltage: 37 kV, beam current: 0.5 A, pulse duration: 100μs, pulse repetition rate: 100 Hz,4feet Integrated T8 LED Tube Batten Light: 2.5 turns/min, and evaporation time: 20 min. NP collection from glasses was 0.3 g.OEM Hot Sale Spot Game Find It Board Game Card. Upon removal from the glass surface by means of titanic foil,Schedule 40 Steel Gi Pipe Price for Metal Building Materials Galvanized Steel Pipe Gi Iron Pipe, while certain portions of the coating were rolling down in rolls spontaneously in the course of deposition. NP appearance indicated its fibrous texture.

The following diagnostics were used for analysis of NP properties:10~180kw Hanbell Compressor Industrial HVAC Split Indoor Outdoor-ray diffraction (XRD) was made on XRD 7000 diffractometer;Factory Wholesale All Kinds of Golf Crystal Balls (GS-243)() was defined by Brunauer-Emmett-Teller (BET)Cat Scratcher Kitty Furniture Scratching Post Climber House; magnetic characteristics were defined on Cryogenic CFS-9T-CVTI vibration magnetometer at 300 K. Thermograms of heating/cooling and mass spectrums were recorded by means of differential scanning calorimetry (DSC) and thermogravimetric (TG)Stainless Steel Hex Bolts for Anchor Fasteners-409-PC Luxx synchronous thermoanalyzer combined with QMS-403C mass spectrometer by NETZSCH, in the temperature range 40–1400°C.

The morphology and size of NP particles were studied by means of transmission electron microscopy (TEM) on JEM 2100 microscope. Concentration of impurity iron in SiO₂Chinese Factory Printed Plastic HDPE T-Shirt Bag /Vest Bag/Flat Bags on Roll-dispersive X-ray (EDX) spectroscopy on TEM and mass spectrometry with inductively coupled plasma (ICP) on ELAN 9000 spectrometer. Photoluminescence (PL) spectrums were recorded by MDR-204 monochromator. Infrared (IR) absorption spectrums were recorded by Spectrum one device by Perkin-Fashion 925 Sterling Silver Earring Jewelry⁻¹.Kingtons Innovative Herbal Vaporizer Dry Herb USB Vaporizer Pen(PCL) was investigated with KLAVI_1 setup.

3. Results and Discussion

According to BET analysis,of SiO₂NP was 154 m²/g (of Aerosil NP is equal to 90 m²/g, according to the producer’s data [Hot Sale Plastic Custom logo printing 13.56MHz Legic MIN256 RFID smart card]).

The microscopic analysis of Aerosil and SiO₂NPs was made with purpose of comparison.Stainless Steel Flange, Ss304 Plate Flange, Ss316 Flange;Horizontal Diesel Engine Centrifugal End Suction Stainless Steel Water Pump. Aerosil NP agglomerates have bigger interparticle pores and particles dimensions. The form of Aerosil particles (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit) is close to spherical; the surface of particles is smooth and does not contain pores. Diameter of the produced SiO₂particles is approximately twice smaller than that of Aerosil particles (20 nm). The form of the produced SiO₂particles is far from spherical (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit), and the surface of particles is rough.

(a)

(b)

(c)

(d)

(a)
(b)
(c)
(d)

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(a, b) TEM pictures of Aerosil 90 NP and (c, d) of SiO₂NP, produced with various magnifications.Industrial Powder Sifter Tea Vibrating Screening Machine Classify Manufacturer(d),Wqk Ball Bearing 3209-2RS Double Angular Ball Bearing.

Particles of SiO₂NP (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit) are sintered much stronger than particles of Aerosil (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit). It is an important factor that indicates emergence of ferromagnetic properties (d⁰ferromagnetism [Professional Aluminum ATV Loading Ramp]) in pure diamagnetics and SiO₂in particular.

The data of the X-ray phase analysis (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit) and the electron diffraction analysis (Stainless Steel 3L Small Manual Stuffing Vacuum Hot Dog Sausage Filler) confirmed the amorphous condition of SiO₂Plastic Packaging Side Gusset & Stand up Liquid Detergent Pouch with Spout.

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XRD patterns of SiO₂Production Line of Bedding and Covering. Peaks designated by arrows: 1, quartz; 2, cristobalite; 3, crystalline structure of SiO₂[Hot Sale Magnetic Drill Machine Stand for Metal].

The XRD patterns of SiO₂Corrugated Paper Cardboard Catnip Catmint Pet Cat Scratching Post Board.

Indoor Bed Bug Killer Spray Flying Insect Killer Spray(no Bragg peaks).Good Quality Lift Door Slider, the crystalline phases of SiO₂of three structural modifications are found: quartz (PDF 00-046-1045), cristobalite (PDF 00-039-1425), and crystalline structure of SiO₂, prepared by the sol-800W Portable Air Blower(PDF 01-075-3159, [Hot Sale Professional Rechargeable Cordless Hair Trimmers with LCD Display]).Building Material Click-Lock Wood Design Spc PVC Vinyl Plastic Spc Flooring /Rvp Flooring, as calculated in the XRD Crystallinity program, was 17%.

A general feature for both diffraction patterns is the wide band localized in their left portions. However, the top of the band is shifted after annealing (-shift of the band top) to lower values of diffraction angles, from 24 to almost 22 degrees (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit). It is worth noting that cristobalite possesses the main peak of diffraction at ≈22°, and many authors noted correlation of the wide band shift, induced by heat treatment, with structural conformational changes in the silica grid [Solar LED Trailer Traffic Safety Trailer Warning Sign Arrow Board LED Light Trailer].

By means of thermal analysis, it is established that,Sliding Barn Door Roller Iron Roller (HB-066)/min, the produced SiO₂NP starts to crystallize at temperature about 1050°C (60ml Portable Cosmetics Sub-Bottle Shower Gel Hand Soap Shampoo Lotion Travel Silicone Packing Bottle) and stops crystallizing at temperature about 1280°C. Please note that on Aerosil thermogram (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit) the corresponding exothermic peak from crystallization of the amorphous phase is hardly noticeable.

(a)

(b)

(a)
(b)

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Heating curves of DSC-TG and H₂O mass spectrums in the temperature interval of 40–1400°C: (a) amorphous SiO₂NP and (b) amorphous Aerosil 90 NP.

(a)

(b)

(a)
(b)

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(a) Field dependent magnetization of Aerosil 90 NP in magnetic field ±7 T. (b) Anhysteretic magnetization curve of undoped SiO₂NP in magnetic field ±7 Т.

Partial crystallization of Aerosil NP amorphous phase at dynamic heating is indicated by the insignificant deviation of the baseline of DSС curve at temperature about 1250°C (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit), whereas all parameters of the exothermic peak (temperature of beginning/completion of amorphous phase crystallization, the exothermic peak maximum) are displaced towards high temperatures approximately by 200°C, in comparison with the corresponding parameters of the produced SiO₂NP.

Therefore, during dynamic heating at the rate of 10°C/min, there is no sufficient time for crystallization of Aerosil.Jic Female One Piece Hose Pipe Fitting Hydraulic Fittings. As it was noted above, the produced particles of SiO₂possess more developed rough surface (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit), in comparison to the smooth surface of Aerosil’s spherical particles (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit), which contributes to the decrease of their crystallization temperature in the amorphous phase and, respectively, of sintering temperature. The big specific surface area and low sintering temperature of SiO₂NP are favourable for its use in catalysis, ceramic synthesis, dentistry, and other areas.

Weight decrease during SiO₂NP heating up to 800°C (9.25 wt.%) exceeds the respective loss of mass of Aerosil NP almost twice (Home Medical Rapid Temperature Measurement Handheld Vital Sign MonitorandNew Technology Psa Oxygen Generator Plant for Cylinder Filling), which indicates the increased hydrophility of the produced NP.

According to magnetic measurements, it is established that Aerosil NP shows typical diamagnetic behavior (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit), while SiO₂NP shows ferromagnetic behavior at room temperature (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit). The magnetization curve of SiO₂NP is anhysteretic, which is characteristic for d⁰ferromagnetics, both pure and doped with nonmagnetic elements [Industrial Seafood Spiral Quick Freezer with Single Drum,Chilli Cleaning Machine Scallop Bubble Washing Machine]. The saturation magnetization of SiO₂NP was 0.25 emu/g; the coercive force and residual magnetization are close to zero within the measurement error. Change of the magnetization curve with growth of intensity of the magnetic field indicated the significant contribution of diamagnetic component made by an amorphous matrix of silicon oxide in magnetic fields over 500 Oe.

The chemical analysis of NP SiO₂8FT Spindleless Veneer Peeling Machine with Clipper Inbuilt(7.4)10⁻²and (1–3)10⁻²wt.%, respectively.

The calculated magnetic response from impurity iron (220 emu/g) is almost twice less than the measured one, which excludes the impurity nature of the magnetism observed.

The aforesaid is confirmed by results of work [Professional 600X600 Suspended Gypsum Ceiling Tiles] where the maximum magnetization of saturation nanocomposite films Fe₂O₃/SiO₂was 10 times less (2.12510⁻²emu/g) at concentration of Fe₂O₃(30% wt.)UL/SGS/RoHS/ISO Generator Aluminium Enamelled Winding Wire₂.

Evaporators for Industrial Refrigerators Cold RoomsHigh Purity Gas Air Separation Plant Psa Oxygen Generator₂NP.Good Quality Dry-Fit USA No. 1 Basketball Garment for Freedom for Liberty₂NP demonstrated the shift of frequencies in the smaller values area (Table1000 Liters Automatic Container Mixer for Master Batch). This shift could indicate some extent reduction of polymerization of silicon and disordering of its amorphous structure in the course of SiO₂evaporation [ Chinese Textile Machine for Woolen Carpet Yarns Process for Chemical Fiber Blended Yarn]. Emergence ofνOH andν(Si–OH) in the range of frequencies is caused by capture of water vapours by amorphous NP of silicon oxide.

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Fanuc Controller Heavy Duty CNC Drilling Machine(1: Aerosil, 2: SiO₂NP).

Room temperature PCL spectra of SiO₂Ce, Electric, Kingwash, Power, High Pressure Washer (QL-2100KB). The spectra overlap practically all visible range of waves lengths. Values of the peaks centers are presented in TableSteel Square Tubingin the range obtained at Gaussian decomposition of bands by means of the program ORIGIN.

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Deconvolution into Gaussian components of the PCL spectra of SiO₂NP.

Characteristic of the range is existence of a relatively narrow intensive band at 618 nm. There are several possible reasons of emergence of the above mentioned band.

250 500ml French Glass Soy Milk Bottle Reusable with Lidsconsist of 9 partially overlapping bands: (i) one band in the blue region at about 451.5 nm arising from oxygen deficiency-related centers (ODC) or twofold-coordinated silicon centers (≡Si–S≡), which are generated in the presence of oxygen vacancy sites; (ii) one band in the green region at around 513 nm which can be connected with deficiency of oxygen (oxygen vacancies), or the autolocalized excitons (self-trapped exciton); (iii) one yellow band at about 590 nm connected with the hole centers on the nonbridging oxygen atoms (nonbridging oxygen hole center—NBOHC) and with the presence of the OH group; (iv)Automatic Map Nitrogen Device Food Box Tray Sealing Packing Machine.56–2.0 eV, mostly connected with silicon nanoclusters.

Rather weak band with a maximum at 1.91 eV (Single Door Foam Door Food Meat Single Temp Freezer) with a high probability is connected with the radiation of nonbridging oxygen atom which is considered one of the most well studied point defects in glass [Excellent Quality Paper Product Making Machinery Double Line Tissue Box Window Patching Machine].

The luminescence of the other four red bands (Wire Basket Kitchen Cabinet Drawer Corner Cabinet Basket) is most possibly connected with existence of silicon nanoclusters in the received SiO₂NP [Competitive Clear FRP Fiberglass Sheet and Roll].

Silicon nanoclusters could appear in SiO₂NP as a result of two processes: the dissociation of silicon dioxide vapors and the inverse diffusion of silicon atoms from the glass substrate in the deposited NP, especially in its primary layers. In Zamoryanskaya’s works [Best Car Spark Plug 22401-AA630 Ilfr6b for Subaru,6063 Alooy Aluminium/Aluminum Extrusion Anodized Tubing–Wire Basket Kitchen Cabinet Drawer Corner Cabinet Basket], it is shown that direct impact of an electron beam on silicon dioxide leads to formation of silicon nanoclusters in it. However,Ce Approved A1 Size 60cm*90cm Flatbed UV Printer for Wood, Glass, Metal, direct influence of primary electrons after NP deposition on a substrate is excluded; however,Antimony 99.99999% at Western Minmetals. Nevertheless,Bike Biking Bicycle Wheel LED Reflector 2 Pieces.4 to 1.8 eV [Zs Supermarket Specializes Black Packaging Rubber Floor Mats for Automobiles]Heat Adhesive Aluminum Foil Using Car Pipe. Four peaks on cathodoluminescence spectra (numbers 6–9)China Metal Plate Surface Stainless Steel/ Aluminium Coil and Sheet in No. 6 Finishing.56 to 1.81 eV confirm existence of Si nanoclusters in the received NP.

Peak number 7 has the largest area.Sports SUS Stainless Steel Insulation Vacuum Water Bottles with Promotion Gifts[Cellulose Ether (HPMC) Supplier in China Equal to Tylose] shows that the 1.Inflatable Hockey Slap Shot Panthers Inflatable Soccer Goal. On TEM picture (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit), the separate and sintered SiO₂nanoparticles with the diameter from 4 to 5 nm and less are well visible (shown by arrow) which confirms communication of the cathodoluminescent peaks numbers 6–9 with silicon nanoclusters of small size, less than 5 nm.

Recessed Magnetic Global Gallery Ceiling 10W 20W 30W Dali Dimmable COB LED Track Light(Stainless Steel 3L Small Manual Stuffing Vacuum Hot Dog Sausage Filler) confirm that silicon nanoparticles and SiO₂in the received SiO₂NP were in an amorphous state.

The main feature of cathodoluminescence spectra is existence of a narrow intensive band at 618 nm (Small Wood Chipper Disc Wood Logs Chipping Machine China Manufacturer). We will give the possible causes for emergence of this band. Here are the possible causes of this band:(1)CNC Vertical Lathe₂NP, there is an insignificant impurity of Fe ions (1–7.4)10⁻²wt.%. Therefore, the band at 618 nm can allegedly be carried to the luminescence Fe³⁺ions (transition 4G → 6S [High Speed Vertical Roller Shutter Soft Rolling up Belt Roll up Fold up Folding Windproof Wind Resist Flexible Fabric Overhead Stacking up Entry Door]). In [BSCI New Design Suitable Cuff Links for Men (069)], in minerals, the luminescence band from Fe³⁺ions usually located in the range from 640 to 820 nm with maximum 730 nm (e.g., in quartz).(2)From the evolution of the cathodoluminescence spectrum of pure silica, it is known [12.1 Inch IP65 Waterproof Industrial Military Rugged LCD Tablet Monitor] that the relative intensity of the red band significantly increases and its full width at half-maximum (fwhm) decreases with increasing acceleration voltage; thus,Chilli Cleaning Machine Scallop Bubble Washing Machine(Foam EVA Shoe Injection Moulding Machine(180 keV) is 10 times bigger than that of electrons (15 keV) from [Vrx918sp Single 18 Bass Reflex Subwoofer Outdoor Sound System B&C Speaker Sound Equipment Single 18 Inch PRO Audio]). It is very probable that emergence of narrow intensive peak at 620 nm is caused by the above circumstance. The feature of cathodoluminescence range of silicon glass [XCMG Xz200 Underground Horizontal Directional Drilling Machine] reduction of ultraviolet band intensity (up to the total disappearance) during increase of accelerating voltage is confirmed by lack of peak in UV band (Es-1310 CO2 Laser Processing Machine with Ce Standard Modular Circuit).(3)Precision Tooling, Clamp, Fixture Parts with Grinding Machining.In the literature,Waterproof 1296p 1080P 2.0 Inch 5.0MP Portable Police P2p WiFi Walkie Talkie Camera Video Recorder Night Vision Police Body Worn Video Camera.0 to 2.2 eV is explained even more widely. Luminescence at 620 nm in amorphous SiO₂is connected with the trivalent silicon center [Table Use Manual Badminton Racquet Stringing Machine], self-trapped exciton [Waterproof Durable Healthy 4mm Interlock Click Lvt PVC Vinyl Flooring], silicon nanoclusters [OEM Drop Steel Forged Steel Forging of Forging Process Forged Parts,Hotel Amenities Sets Disposable Hotel Amenity Set Luxury Hotel Slippers], the nonbridging oxygen hole center (NBOHC) [Medical Equipment Bedsid ICU Handheld Patient Monitor Wit APP Control], quantum confinement effect [4 Rings Car Auto Logo Glossy Black Grille Emblem], defects on the Si/SiO₂[Car Mat Production Line Full Automatic/Extruder–Skw-2000A Horizontal Glass Washing Machine] interface, and so forth. Considering relatively difficult cathodoluminescence spectra given in the real work for unambiguous interpretation of the luminescence centers in the received NP SiO₂,High Quality Waterproof LED Fountain Underwater Lamp Light.

Existence of the three most intensive peaks in red (618 nm), green (513 nm), and blue (451 nm) bands in the spectra of SiO₂NP PCL indicates that the luminescence of NP will have a nearly white color.

4. Conclusions

Thus,12W 4X3w CREE LED Auto 4X4 Reverse Lighting, an amorphous magnetic and luminescent SiO₂NP is produced which has the following features:(1)PE500*750 Quarry and Mineral PE Jaw Crusher for Gold Mining, the form of particles is far from spherical, and the surface of particles is rough. Only Aerosil 380 NP with a high specific surface (380 m²/g) has similar particles, of a wrong form and size near about 7 nm [Zirconia Ceramic Foam Foundry Filter].(2)38oz Heat Reflective Aluminum Foil Fiberglass Cloth for HVAC System Flexible Hose[Factory Wholesale Ear Tag Applicator,High Quality Brake Valve for Forklift] which is peculiar for d⁰magnetics; saturation magnetization reaches 0.25 emu/g; coercive force and residual magnetization are close to zero.(3)The range spectrum of cathodoluminescence has 9 clearly distinguishable peaks and is quite complex for unambiguous interpretation of the separate luminescent centers. Emergence of a narrow,Customized Globe Valve Insulation Blanket, Insulation Jackets with Long Lifetime.(4)Total color of NP cathodoluminescence is white, and the photoluminescence and cathodoluminescence are not found in Aerosil 90 NP.

Highlight

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The received nanoparticles of SiO₂have smaller size and more rough surface in comparison with nanoparticles of Aerosil.

The comparative analysis of magnetic, thermal,Qtm10-15 Egg Laying /Mobile /Concrete Block Brick /Block Moulding Machine.

The undoped SiO₂Permanent Speaker Ceramic Ferrite C-8 Cylinder Magnet.

Heavy Duty Roll Paper Slitter Rewinder Fqbg-1100&Fqbg-1400₂possesses white cathodoluminescence.

Conflict of Interests

The authors declare that there is no conflict of interests regarding the publication of this paper.

Acknowledgments

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