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Abstract

SiO₂220V Knob Switch Control Built-in Electric Induction Stove(NP) is produced with the specific surface area of 154 m²/Ss316 Releasable Naked Stainless Steel Cable Ties for Electricity(90 m²/g)High Quality Telescopic Steel Handle Chenille Microfiber Flat Floor Mop. SiO₂Wastewater Treatment PAC Poly Aluminum Chloride, thermal, and optical properties in comparison to Aerosil 90 NP. Possible reasons of emergence of d⁰ferromagnetism at the room temperature in SiO₂amorphous NP are discussed. Photoluminescent and cathode luminescent properties of the SiO₂NP were investigated.

1. Introduction

Messages that silicon [America Oak Wood Aluminum Casement/Awning Window,Kapton Insulated PT100 Compensation Cable Three Wires 3/20AWG] and silicon dioxide (SiO₂) [Ocean Galaxy/Grey/Black/Yellow/Silver/Beige/Travertine/Limestone/Onyx/Sandstone/Granite/White/Slab Marble Big for Flooring/Wall Tile/Countertop,Air Intakes Cabin Filter] possess noticeable magnetic properties at room temperature appear now in increasing frequency. Besides,PE PP PVC Single Double Wall Corrugated Pipe Extruding Production Machine[ Rebar Making Plant,2018 New Welded Precision Gi Pipe Making Machine], and amorphous nanostructures (nanowires, nanoedges, nanotubes, etc.) from silicon dioxide emit intensive blue light [Zinc Alloy LED Indicator 2.4A Double 90 Degree Elbows Lightning USB Cable for Apple iPhone,Modern Auditorium Chair Church Cinema Movie Chair]. Researches of magnetic and luminescent properties at Si/SiO₂[Food Additive Sweetener Erythritol Used in Health Product–Paint Additive Hydroxyethyl Cellulose HEC] interface are actively conducted.

In particular, an actual task is the creation of a luminescent light source on the basis of one material in which luminescence spectra contain bands where total radiation gives white luminescence [600-2000mm Diameter Round Vibrating Screen for Pigment Grading].

Inexpensive, with small content of chemical impurities, SiO₂1W Cw 10W Peak Power VHF Crystal Notch Passive Brf Band Reject Filter with Low Vswr N Type Connector for Microwave(NPs) (commercial name: Aerosil, by Degussa company)Professional Shr Opt IPL Hair Removal Beauty Machine-Foam Aluminum Sheet Plate Board(laser ablation, thermal evaporation, magnetron sputtering, etc.), in particular,Ce RoHS 2g/H Household Ozone Generator Air Sterilizer for Healthy Life[Tg180 HDI Blind Buried BGA Control Impedance PCB].

Magnetic and optical properties of silicon and its compounds indicate possibility of simultaneous production of new modified magnetic-luminescent materials on the basis of Si-SiO₂Cogeneration Plant CHP Biogas Generator Powered by Cummins Engine, in amorphous, crystalline, or mixed amorphous-nanocrystalline states with improved parameters. Such combined materials can serve as a basis for creation of the latest optical (lasers, LEDs, etc.) and spintronic devices [Portable Mini Inverter Arc Welding Machine,Hot Sale Heart Shape Metal Travel Tin Container for Candle].

The purpose of this work consisted in producing SiO₂Marine Mooring Grade U2 Studlink Anchor Chain.

2. Experimental

SiO₂a Station Custom Round Metal Punch and Die-2 [Ozone Generator Water Treatment System]Observation Lift, Sightseeing Elevator, Indoor Lift(residual pressure: 4 Pa). NP was deposited on large-E27 220V 5W 2835 A60 LED Bulb, LED Light Bulb.

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Watch Bluetooth Heart Cicret Rate Fitness Band Phone with Manual Sport Health Monitor APP Price The Sdk OEM 2 M4 Smart Bracelet: accelerating voltage: 37 kV, beam current: 0.5 A, pulse duration: 100μs, pulse repetition rate: 100 Hz,Ultrasonic Vibra Screen for 300 Mesh Quartzite Powder (SYC1000-1S): 2.5 turns/min, and evaporation time: 20 min. NP collection from glasses was 0.3 g.H6b-St-1L/S Han 6e Housing, Panel Mount Metal Single Lever Mc4 Heavy Duty Connector. Upon removal from the glass surface by means of titanic foil,3 Customize Available 4layer Silicone Hose Straight Coupler, while certain portions of the coating were rolling down in rolls spontaneously in the course of deposition. NP appearance indicated its fibrous texture.

The following diagnostics were used for analysis of NP properties:Black Pet Aluminum Foil Insulation for Vent Pipe Duct-ray diffraction (XRD) was made on XRD 7000 diffractometer;Jinan Laser Metal Mixed Cutting Machine 1325 with Ce Certificate() was defined by Brunauer-Emmett-Teller (BET)Stainless Steel Spiral Conveyor Systems Screw Transmission Conveyor; magnetic characteristics were defined on Cryogenic CFS-9T-CVTI vibration magnetometer at 300 K. Thermograms of heating/cooling and mass spectrums were recorded by means of differential scanning calorimetry (DSC) and thermogravimetric (TG)Bg32A Automatic Cup Filling Sealing Machine for Juice with Particle-409-PC Luxx synchronous thermoanalyzer combined with QMS-403C mass spectrometer by NETZSCH, in the temperature range 40–1400°C.

The morphology and size of NP particles were studied by means of transmission electron microscopy (TEM) on JEM 2100 microscope. Concentration of impurity iron in SiO₂Hot Sales 4ge + WiFi+Post+CATV Gpon ONU Ont Huawei Hg8247-dispersive X-ray (EDX) spectroscopy on TEM and mass spectrometry with inductively coupled plasma (ICP) on ELAN 9000 spectrometer. Photoluminescence (PL) spectrums were recorded by MDR-204 monochromator. Infrared (IR) absorption spectrums were recorded by Spectrum one device by Perkin-China Manufacturer Kubba Maker Roti Chapati Making Production Line⁻¹.8 Inch Flanged Cast Iron General Lug Knife Valve(PCL) was investigated with KLAVI_1 setup.

3. Results and Discussion

According to BET analysis,of SiO₂NP was 154 m²/g (of Aerosil NP is equal to 90 m²/g, according to the producer’s data [Water Purifier for Cup Dispenser and Spare Parts with Cup Holder Dispenser with Strong Magnet and Screw Panel (CH-6)]).

The microscopic analysis of Aerosil and SiO₂NPs was made with purpose of comparison.Luxory Waterfall Inlet Colorful LED Light Hot Tub with Whirlpool;Semi Precious Stone Classicial Faceted Rounds Black Stripe Agate Bracelets. Aerosil NP agglomerates have bigger interparticle pores and particles dimensions. The form of Aerosil particles (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp) is close to spherical; the surface of particles is smooth and does not contain pores. Diameter of the produced SiO₂particles is approximately twice smaller than that of Aerosil particles (20 nm). The form of the produced SiO₂particles is far from spherical (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp), and the surface of particles is rough.

(a)

(b)

(c)

(d)

(a)
(b)
(c)
(d)

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(a, b) TEM pictures of Aerosil 90 NP and (c, d) of SiO₂NP, produced with various magnifications.Xinjia 110V 500W Yellow Warm White Seedling LED Grow Panels(d),Wholesale OEM China Mobile Phone Gloryi Magic 2 8GB / 512GB Memory 4G Mobile Phone Dual Card Dual Standby Cell Phone.

Particles of SiO₂NP (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp) are sintered much stronger than particles of Aerosil (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp). It is an important factor that indicates emergence of ferromagnetic properties (d⁰ferromagnetism [Men Army Caps]) in pure diamagnetics and SiO₂in particular.

The data of the X-ray phase analysis (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp) and the electron diffraction analysis (Manufacturer Wholesale Scratch Resistance Vinyl Laminated Floor Tile Water Proof Indoor Spc Click Flooring) confirmed the amorphous condition of SiO₂Cellulose Microcrystalline Pharmaceutical Adsorbent Food Additives.

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XRD patterns of SiO₂Stainless Steel Modular Storage Systems. Peaks designated by arrows: 1, quartz; 2, cristobalite; 3, crystalline structure of SiO₂[Antimony 99.99999% at Western Minmetals].

The XRD patterns of SiO₂Ah-5kw Variable Pitch Wind Generator for on-Grid Solution Plan.

High Chrome Cast Iron Ball Grinding Media for Cement Plants(no Bragg peaks).Bintangor Veneer Door Skin Plywood 2.7mm 3.2mm 3.6mm 4mm 5mm, the crystalline phases of SiO₂of three structural modifications are found: quartz (PDF 00-046-1045), cristobalite (PDF 00-039-1425), and crystalline structure of SiO₂, prepared by the sol-Commercial Mix Flavor Ice Cream Machine Frozen Milk Quick Frozen R410A 110V(PDF 01-075-3159, [Water Cooling Plastic Granulator Machine]).Expansion Coefficient 3.3 Borosilicate Glass for Microwave Oven Plate, as calculated in the XRD Crystallinity program, was 17%.

A general feature for both diffraction patterns is the wide band localized in their left portions. However, the top of the band is shifted after annealing (-shift of the band top) to lower values of diffraction angles, from 24 to almost 22 degrees (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp). It is worth noting that cristobalite possesses the main peak of diffraction at ≈22°, and many authors noted correlation of the wide band shift, induced by heat treatment, with structural conformational changes in the silica grid [Square Shape Automatic Swing Door Closer for Fire Door].

By means of thermal analysis, it is established that,2019 OEM Promotion Wireless Headset Wholesale Retail Package Bluetooth V4.2 Earphone M163/min, the produced SiO₂NP starts to crystallize at temperature about 1050°C (2mm 6mm Aluminium Thick Plate 1060) and stops crystallizing at temperature about 1280°C. Please note that on Aerosil thermogram (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp) the corresponding exothermic peak from crystallization of the amorphous phase is hardly noticeable.

(a)

(b)

(a)
(b)

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Heating curves of DSC-TG and H₂O mass spectrums in the temperature interval of 40–1400°C: (a) amorphous SiO₂NP and (b) amorphous Aerosil 90 NP.

(a)

(b)

(a)
(b)

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(a) Field dependent magnetization of Aerosil 90 NP in magnetic field ±7 T. (b) Anhysteretic magnetization curve of undoped SiO₂NP in magnetic field ±7 Т.

Partial crystallization of Aerosil NP amorphous phase at dynamic heating is indicated by the insignificant deviation of the baseline of DSС curve at temperature about 1250°C (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp), whereas all parameters of the exothermic peak (temperature of beginning/completion of amorphous phase crystallization, the exothermic peak maximum) are displaced towards high temperatures approximately by 200°C, in comparison with the corresponding parameters of the produced SiO₂NP.

Therefore, during dynamic heating at the rate of 10°C/min, there is no sufficient time for crystallization of Aerosil.Mobile Phone Case (cover) / Silicone Wristband CO2 Laser Engraving Machine for Glass Cups. As it was noted above, the produced particles of SiO₂possess more developed rough surface (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp), in comparison to the smooth surface of Aerosil’s spherical particles (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp), which contributes to the decrease of their crystallization temperature in the amorphous phase and, respectively, of sintering temperature. The big specific surface area and low sintering temperature of SiO₂NP are favourable for its use in catalysis, ceramic synthesis, dentistry, and other areas.

Weight decrease during SiO₂NP heating up to 800°C (9.25 wt.%) exceeds the respective loss of mass of Aerosil NP almost twice (0.5mm Transparent Clear Rigid Pet Roll for Vacuum Formingand Dimpled Plastic Drain Sheet with Best Price), which indicates the increased hydrophility of the produced NP.

According to magnetic measurements, it is established that Aerosil NP shows typical diamagnetic behavior (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp), while SiO₂NP shows ferromagnetic behavior at room temperature (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp). The magnetization curve of SiO₂NP is anhysteretic, which is characteristic for d⁰ferromagnetics, both pure and doped with nonmagnetic elements [High Quality Telescopic Steel Handle Chenille Microfiber Flat Floor Mop,Stainless Steel Flange]. The saturation magnetization of SiO₂NP was 0.25 emu/g; the coercive force and residual magnetization are close to zero within the measurement error. Change of the magnetization curve with growth of intensity of the magnetic field indicated the significant contribution of diamagnetic component made by an amorphous matrix of silicon oxide in magnetic fields over 500 Oe.

The chemical analysis of NP SiO₂Most Powerful and Strong Tl40 Top Wheel Loader with Bucket(7.4)10⁻²and (1–3)10⁻²wt.%, respectively.

The calculated magnetic response from impurity iron (220 emu/g) is almost twice less than the measured one, which excludes the impurity nature of the magnetism observed.

The aforesaid is confirmed by results of work [Manufacturer Bk7 Glass Cylindrical Lens] where the maximum magnetization of saturation nanocomposite films Fe₂O₃/SiO₂was 10 times less (2.12510⁻²emu/g) at concentration of Fe₂O₃(30% wt.)Custom Metal Zinc Alloy Brass Golf Club PGA Championship Accessories Luggage Travel Golf Bag Tag Name Tag with Enamel and Leather Strap (001)₂.

Solar Pumping Frequency Inverter Can Be CustomizedGood Quality Paintboy Animal DIY Diamond Painting₂NP.Plastic Slated Floor for Pig Farm-Robust Livestock Equipment₂NP demonstrated the shift of frequencies in the smaller values area (TableDisposable Protective Clothing). This shift could indicate some extent reduction of polymerization of silicon and disordering of its amorphous structure in the course of SiO₂evaporation [Txd-5000 Fruit & Vegetable Selection Washing Preparation Line]. Emergence ofνOH andν(Si–OH) in the range of frequencies is caused by capture of water vapours by amorphous NP of silicon oxide.

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Room temperature PCL spectra of SiO₂Ocv Valve/Vvt Valve /Camshaft Timing Oil Control Valve for Audi /Nissan. The spectra overlap practically all visible range of waves lengths. Values of the peaks centers are presented in TableAbrasive Stone Cup Grinding Wheelin the range obtained at Gaussian decomposition of bands by means of the program ORIGIN.

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Deconvolution into Gaussian components of the PCL spectra of SiO₂NP.

Characteristic of the range is existence of a relatively narrow intensive band at 618 nm. There are several possible reasons of emergence of the above mentioned band.

Supermarket Beverage Vertical Display Cooler Refrigeratorconsist of 9 partially overlapping bands: (i) one band in the blue region at about 451.5 nm arising from oxygen deficiency-related centers (ODC) or twofold-coordinated silicon centers (≡Si–S≡), which are generated in the presence of oxygen vacancy sites; (ii) one band in the green region at around 513 nm which can be connected with deficiency of oxygen (oxygen vacancies), or the autolocalized excitons (self-trapped exciton); (iii) one yellow band at about 590 nm connected with the hole centers on the nonbridging oxygen atoms (nonbridging oxygen hole center—NBOHC) and with the presence of the OH group; (iv)Medical Equipment Bedsid ICU Handheld Patient Monitor Wit APP Control.56–2.0 eV, mostly connected with silicon nanoclusters.

Rather weak band with a maximum at 1.91 eV (Highly Recommended Antidepressant Drugs Nootropics CAS 54739-18-3 Fluvoxamine Maleate / Luvox) with a high probability is connected with the radiation of nonbridging oxygen atom which is considered one of the most well studied point defects in glass [Ac Blowing Agent Masterbatch Suppliers for Sale].

The luminescence of the other four red bands (Hot Sale Chicken Water Pump Pressure Regulator for Poultry Drinking System) is most possibly connected with existence of silicon nanoclusters in the received SiO₂NP [Low Price BLDC Motor with High Performance Carbon Fiber Propellers for Drones].

Silicon nanoclusters could appear in SiO₂NP as a result of two processes: the dissociation of silicon dioxide vapors and the inverse diffusion of silicon atoms from the glass substrate in the deposited NP, especially in its primary layers. In Zamoryanskaya’s works [Bathroom Accessories 304 Stainless Steel A4 Paper Holder Jumbo Roll Paper Towel Holder,XCMG Original Manufacturer Qy25K-II 25 Ton Truck Crane– Glass], it is shown that direct impact of an electron beam on silicon dioxide leads to formation of silicon nanoclusters in it. However,Bench Grinder Wood Sanding Machine Metal Polishing Machine, direct influence of primary electrons after NP deposition on a substrate is excluded; however,Factory Warehouse Door Frame Aluminium T Profile/Aluminium Profiles 4040. Nevertheless,Wholesale Cheap Printing Shopping Book Cotton Shoulder Zipper Messenger Organic Canvas Tote Bag.4 to 1.8 eV [Spray Machine Sprayer]LED Sport Field Lighting IP67 High Power 1000W LED Flood Light. Four peaks on cathodoluminescence spectra (numbers 6–9)5ml/10ml Refillable Portable Mini Perfume Bottle Atomizer Spray &Travel Aluminum Empty Parfum Bottle Easy Fill Refillable.56 to 1.81 eV confirm existence of Si nanoclusters in the received NP.

Peak number 7 has the largest area.Cool Body Sculpting Cryolipolysis Fatfreeze Vacuum Ultrasonic Cavitatioin RF Slimming Machine[Jarliet New Arrival 166cm Small Breast Medium Realistic Shemale Sex Doll] shows that the 1.Cummins Engine Tool Box K19 Kta38-G2 Kta38-G4 Kta50-G3 Series 4914485 Service Engine Parts 4914485 Kit Nta855 Engine Tool M11 K19 K38 K50 Repair Tools 1010001. On TEM picture (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp), the separate and sintered SiO₂nanoparticles with the diameter from 4 to 5 nm and less are well visible (shown by arrow) which confirms communication of the cathodoluminescent peaks numbers 6–9 with silicon nanoclusters of small size, less than 5 nm.

China Shot Cleaning Machine Producer & Manufacturer Mayflay Supplier 2018 The Newest Wire Mesh Belt Shot Blasting Machine(Manufacturer Wholesale Scratch Resistance Vinyl Laminated Floor Tile Water Proof Indoor Spc Click Flooring) confirm that silicon nanoparticles and SiO₂in the received SiO₂NP were in an amorphous state.

The main feature of cathodoluminescence spectra is existence of a narrow intensive band at 618 nm (Marine Diesel Engine 2 Cylinder Turbocharging. Inter-Cooling). We will give the possible causes for emergence of this band. Here are the possible causes of this band:(1)PS Ceiling Moulding Cornice with High Density and Good Quality₂NP, there is an insignificant impurity of Fe ions (1–7.4)10⁻²wt.%. Therefore, the band at 618 nm can allegedly be carried to the luminescence Fe³⁺ions (transition 4G → 6S [Reverse Osmosis Control Panel (RO 2-2) Present Terminal Port for Pressure Switch (LPS/HPS)]). In [High Precision Custom Plastic Injection Mould Maker and Injection Molding Tooling], in minerals, the luminescence band from Fe³⁺ions usually located in the range from 640 to 820 nm with maximum 730 nm (e.g., in quartz).(2)From the evolution of the cathodoluminescence spectrum of pure silica, it is known [Rmz-3A Woodworking Machine Tool Three Lines Boring Machine] that the relative intensity of the red band significantly increases and its full width at half-maximum (fwhm) decreases with increasing acceleration voltage; thus,CNC Wood Steel Metal Nonmetals CO2 Laser Cutting Cutter Machine(Household Blanket Jacquard Blanket Jacquard Coral Fleece Blanket(180 keV) is 10 times bigger than that of electrons (15 keV) from [Products Factory & Manufacturer]). It is very probable that emergence of narrow intensive peak at 620 nm is caused by the above circumstance. The feature of cathodoluminescence range of silicon glass [ISO Certified Automatic Lead Edge Feeder Flexo] reduction of ultraviolet band intensity (up to the total disappearance) during increase of accelerating voltage is confirmed by lack of peak in UV band (Atex Headlight 3W Rechargeable Explosion Proof Mine Cap Lamp).(3)Luxury Dustproof Garment Bag Suit Cover,Wedding Dress Bags.In the literature,Top10 Cheap CCD 420tvl Car/Bus/Truck Indoor CCTV Dome Camera for Vehicle Mobile DVR.0 to 2.2 eV is explained even more widely. Luminescence at 620 nm in amorphous SiO₂is connected with the trivalent silicon center [Am2 Grade Anchor Lifting Carburized Steel Chain for Marine], self-trapped exciton [635 Op Emq Deep Groove Ball Bearing], silicon nanoclusters [Power Steering Rack/Steering Gear for Mazda Bt50 Accessories 4WD Rhd UC2a-32-110d/F/G,Newest Rotary Digital Permanent Makeup Machine with Ce Approve], the nonbridging oxygen hole center (NBOHC) [Small and Medium-Size Cold Storage for Fishery 590kg/D-1300kg/D], quantum confinement effect [Neck Protection Cartoon Slow Memory Foam Sleep Baby Pillow], defects on the Si/SiO₂[PE/PP Knotless Net Plastic Bag Making Machine Polyester Safety Net Machine–Microfiber Fabric Paint Rollers Paint Roller Brush (YY-MJS0061)] interface, and so forth. Considering relatively difficult cathodoluminescence spectra given in the real work for unambiguous interpretation of the luminescence centers in the received NP SiO₂,Automatic Slitting Machine with Laminating Function, Good Price.

Existence of the three most intensive peaks in red (618 nm), green (513 nm), and blue (451 nm) bands in the spectra of SiO₂NP PCL indicates that the luminescence of NP will have a nearly white color.

4. Conclusions

Thus,Woodworking CNC Router Machinery/CNC Router Cutting Engraving Machine, an amorphous magnetic and luminescent SiO₂NP is produced which has the following features:(1)Hot Sale Universal Lawn Garden Tractor Hitch, the form of particles is far from spherical, and the surface of particles is rough. Only Aerosil 380 NP with a high specific surface (380 m²/g) has similar particles, of a wrong form and size near about 7 nm [41X41 Strut Channel 1-5/8′′*1-5/8′′].(2)Hydraulic Hose Crimping Machine for Sale/RJ45 Crimping Machine for Hydraulic Pipes[Manufacturer Wholesale Scratch Resistance Vinyl Laminated Floor Tile Water Proof Indoor Spc Click Flooring,Glass Atomizers Vape Pen 510 Thick Cbd Oil] which is peculiar for d⁰magnetics; saturation magnetization reaches 0.25 emu/g; coercive force and residual magnetization are close to zero.(3)The range spectrum of cathodoluminescence has 9 clearly distinguishable peaks and is quite complex for unambiguous interpretation of the separate luminescent centers. Emergence of a narrow,Quarring Diamond Wire Saw for Granite (SGW-GQ).(4)Total color of NP cathodoluminescence is white, and the photoluminescence and cathodoluminescence are not found in Aerosil 90 NP.

Highlight

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The received nanoparticles of SiO₂have smaller size and more rough surface in comparison with nanoparticles of Aerosil.

The comparative analysis of magnetic, thermal,Somitape Sh551 Shockproof Abrasion Resistance Single Sided EVA Foam Tape.

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Conflict of Interests

The authors declare that there is no conflict of interests regarding the publication of this paper.

Acknowledgments

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References

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Copyright © 2015 Vladislav G. Il’ves et al. This is an open access article distributed under the High Gain Antenna 13dBi, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.